Different conditions of process and preparation methods to intercalate and exfoliate organoclay in constituents of final nanocomposite, based on polyol or isocyanate have been studied. Different formulations of polyurethane-matrix nanocomposites have been examined by X-ray diffraction (XRD), transmission electron microscopy (TEM), field emission gun scanning electron microscopy (FEGSEM), and rheological measurement. The results obtained from this study provide a good understanding of the relationship between the formulation, processing conditions, and performance. The processing conditions have great effects on the final properties of nanocomposites such as mechanical properties. The results show a high performance nanocomposite systems produced by high strength ultra-sonication in a short time.
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Oak Ridge Natl Lab, Mat Sci & Technol Div, Carbon & Composites Grp, Oak Ridge, TN 37831 USAOak Ridge Natl Lab, Mat Sci & Technol Div, Carbon & Composites Grp, Oak Ridge, TN 37831 USA
Naskar, Amit K.
Keum, Jong K.
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Oak Ridge Natl Lab, Ctr Nanophase Mat Sci & Spallat Neutron Source, Oak Ridge, TN 37831 USAOak Ridge Natl Lab, Mat Sci & Technol Div, Carbon & Composites Grp, Oak Ridge, TN 37831 USA
Keum, Jong K.
Boeman, Raymond G.
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Oak Ridge Natl Lab, Energy & Environm Sci Directorate, Oak Ridge, TN 37831 USA
Michigan State Univ, E Lansing, MI 48824 USAOak Ridge Natl Lab, Mat Sci & Technol Div, Carbon & Composites Grp, Oak Ridge, TN 37831 USA