Atom probe tomography characterization of heavily cold drawn pearlitic steel wire

被引:73
作者
Li, Y. J. [1 ,2 ]
Choi, P. [1 ]
Borchers, C. [2 ]
Chen, Y. Z. [2 ]
Goto, S. [3 ]
Raabe, D. [1 ]
Kirchheim, R. [1 ,2 ]
机构
[1] Max Planck Inst Eisenforsch GmbH, D-40237 Dusseldorf, Germany
[2] Univ Gottingen, Inst Mat Phys, D-37077 Gottingen, Germany
[3] Akita Univ, Dept Mat Sci & Engn, Fac Engn & Resource Sci, Akita 0100852, Japan
关键词
Atom probe tomography; Pearlitic steel wire; Cementite decomposition; Severe plastic deformation; Dislocations; Cell boundaries; SEVERE PLASTIC-DEFORMATION; TRANSMISSION ELECTRON-MICROSCOPY; CEMENTITE DISSOLUTION; SPECIMEN PREPARATION; FE-C; MICROSTRUCTURE; FIB;
D O I
10.1016/j.ultramic.2010.11.010
中图分类号
TH742 [显微镜];
学科分类号
摘要
Atom Probe Tomography (APT) was used to analyze the carbon distribution in a heavily cold drawn pearlitic steel wire with a true strain of 6.02. The carbon concentrations in cementite and ferrite were separately measured by a sub-volume method and compared with the literature data. It is found that the carbon concentration in ferrite saturates with strain. The carbon concentration in cementite decreases with the lamellar thickness, while the carbon atoms segregate at dislocations or cell/grain boundaries in ferrite. The mechanism of cementite decomposition is discussed in terms of the evolution of dislocation structure during severe plastic deformation. (C) 2010 Elsevier B.V. All rights reserved.
引用
收藏
页码:628 / 632
页数:5
相关论文
共 37 条
[1]   Partially amorphous nanocomposite obtained from heavily deformed pearlitic steel [J].
Borchers, Christine ;
Al-Kassab, Talaat ;
Goto, Shoji ;
Kirchheim, Reiner .
MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING, 2009, 502 (1-2) :131-138
[2]   INTERACTION BETWEEN DISLOCATIONS AND INTERSTITIAL ATOMS IN BODY-CENTERED CUBIC METALS [J].
COCHARDT, AW ;
SCHOEK, G ;
WIEDERSICH, H .
ACTA METALLURGICA, 1955, 3 (06) :533-537
[3]   Direct evidence of cementite dissolution in drawn pearlitic steels observed by tomographic atom probe [J].
Danoix, F ;
Julien, D ;
Sauvage, X ;
Copreaux, J .
MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING, 1998, 250 (01) :8-13
[4]   Comment on "Effect of interlamellar spacing on cementite dissolution during wire drawing of pearlitic steel wires" [J].
Gavriljuk, VG .
SCRIPTA MATERIALIA, 2001, 45 (12) :1469-1472
[5]   Application of cold drawn lamellar microstructure for developing ultra-high strength wires [J].
Goto, S. ;
Kirchheim, R. ;
Al-Kassab, T. ;
Borchers, C. .
TRANSACTIONS OF NONFERROUS METALS SOCIETY OF CHINA, 2007, 17 (06) :1129-1138
[6]   MOSSBAUER-EFFECT IN DEFORMED FE-C ALLOYS [J].
GRIDNEV, VN ;
NEMOSHKALENKO, VV ;
MESHKOV, YY ;
GAVRILYUK, VG ;
PROKOPENKO, VG ;
RAZUMOV, ON .
PHYSICA STATUS SOLIDI A-APPLIED RESEARCH, 1975, 31 (01) :201-210
[7]   INVESTIGATION OF CARBIDE PHASE IN STRAINED STEEL BY METHOD OF NUCLEAR GAMMA RESONANCE [J].
GRIDNEV, VN ;
GAVRILYUK, VG ;
DEKHTYAR, IY ;
MESHKOV, YY ;
NIZIN, PS ;
PROKOPENKO, VG .
PHYSICA STATUS SOLIDI A-APPLICATIONS AND MATERIALS SCIENCE, 1972, 14 (02) :689-694
[8]   Atom probe and transmission electron microscopy investigations of heavily drawn pearlitic steel wire [J].
Hong, MH ;
Hono, K ;
Reynolds, WT ;
Tarui, T .
METALLURGICAL AND MATERIALS TRANSACTIONS A-PHYSICAL METALLURGY AND MATERIALS SCIENCE, 1999, 30 (03) :717-727
[9]   Cementite decomposition in heavily drawn pearlite steel wire [J].
Hono, K ;
Ohnuma, M ;
Murayama, M ;
Nishida, S ;
Yoshie, A ;
Takahashi, T .
SCRIPTA MATERIALIA, 2001, 44 (06) :977-983
[10]  
INOUE A, 1977, T IRON STEEL I JPN, V17, P143