Atomic force microscopy studies on liquid inclusions and induced defects of cadmium mercury thiocyanate crystal

被引:7
作者
Jiang, XN [1 ]
Xu, D
机构
[1] Dalian Univ Technol, State Key Lab Mat Modificat Laser Ion & Elect Bea, Dalian 116023, Peoples R China
[2] Shandong Univ, Inst Crystal Mat, State Key Lab Crystal Mat, Jinan 250100, Peoples R China
关键词
cadmium mercury thiocyanate crystal; atomic force microscopy; liquid inclusions; dislocations and cracks; screw dislocation growth;
D O I
10.1002/crat.200310093
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
Liquid inclusions and various defects accordingly induced on a nonlinear optical material of CMTC crystal were investigated by atomic force microscopy. Liquid inclusions are chiefly caused by formation of macrosteps, which result from impurity-induced inhibiting of step growth and meeting of step trains advancing along different directions. Liquid inclusions induce generation of dislocations and even cracks within the crystal by three-dimensional nucleation growth. Liquid inclusions also provide screw dislocation growth sources, leading to formation of spiral hillock trains with ridged tails. Etching experiments reveal circular hollow cores, indicative of screw dislocation growth, and negative crystals resulting from further crystallization in the liquid inclusions.
引用
收藏
页码:767 / 772
页数:6
相关论文
共 18 条
  • [1] CHERNOV AA, 1984, MODERN CRYSTALLOGR 3, V36, P249
  • [2] Study on the micro-crystallization of cadmium mercury thiocyanate (CMTC) crystal for laser diode frequency doubling
    Duan, XL
    Yuan, DR
    Zhong, ZW
    Zhang, JG
    Wang, XQ
    Jiang, XN
    Guo, SY
    Xu, D
    Lu, MK
    [J]. JOURNAL OF CRYSTAL GROWTH, 2001, 233 (1-2) : 312 - 317
  • [3] Atomic force microscopy studies on phase transitions and surface morphology transformation of CMTC crystals
    Jiang, XN
    Xu, D
    Yuan, DR
    Sun, DL
    Lu, MK
    Jiang, MH
    [J]. APPLIED PHYSICS A-MATERIALS SCIENCE & PROCESSING, 2002, 75 (05): : 617 - 620
  • [4] Jiang XN, 2002, CRYST RES TECHNOL, V37, P67, DOI 10.1002/1521-4079(200202)37:1<67::AID-CRAT67>3.0.CO
  • [5] 2-M
  • [6] Formation of small straight steps among large rough steps on the {110} face of cadmium mercury thiocyanate crystal
    Jiang, XN
    Xu, D
    Sun, DL
    Yuan, DR
    Lu, MK
    Zhang, GH
    Fang, Q
    [J]. JOURNAL OF CRYSTAL GROWTH, 2001, 233 (1-2) : 318 - 325
  • [7] Investigation of growth modes of cadmium mercury thiocyanate crystal by atomic force microscopy
    Jiang, XN
    Sun, DL
    Xu, D
    Yuan, DR
    Lu, MK
    Guo, SY
    Fang, Q
    [J]. JOURNAL OF CRYSTAL GROWTH, 2001, 233 (1-2) : 196 - 207
  • [8] Jiang XN, 2001, ACTA CHIM SINICA, V59, P724
  • [9] Recovery of surfaces from impurity poisoning during crystal growth
    Land, TA
    Martin, TL
    Potapenko, S
    Palmore, GT
    De Yoreo, JJ
    [J]. NATURE, 1999, 399 (6735) : 442 - 445
  • [10] In situ atomic force microscopy studies of surface morphology, growth kinetics, defect structure and dissolution in macromolecular crystallization
    Malkin, AJ
    Kuznetsov, YG
    McPherson, A
    [J]. JOURNAL OF CRYSTAL GROWTH, 1999, 196 (2-4) : 471 - 488