Synthesis of [15N3]melamine and [13C3]cyanuric acid

被引:3
作者
Luo, Yong [1 ]
Zhang, Liya [1 ]
Yang, Weicheng [1 ]
Liu, Weixia [1 ]
Lu, Weijing [1 ]
Li, Meihua [1 ]
机构
[1] Shanghai Res Inst Chem Ind, Shanghai, Peoples R China
关键词
isotopically labelled synthesis; N-15; melamine; cyanuric acid; labelled; synthesis; internal standards; CYANURIC ACID; MELAMINE; CATS;
D O I
10.1002/jlcr.1835
中图分类号
Q5 [生物化学];
学科分类号
071010 ; 081704 ;
摘要
This report presents an efficient syntheses of two labelled internal standards [N-15(3)] melamine and [C-13(3)] cyanuric acid with the common substrates [N-15]NH4Cl and [C-13] urea, respectively. Both standards with excellent isotopic and chemical purities were prepared in good yields and could be used as internal standards without further purification.
引用
收藏
页码:171 / 172
页数:2
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