Characterization of spark plasma sintered TiC ceramics reinforced with graphene nano-platelets

被引:40
作者
Thang Phan Nguyen [1 ,2 ]
Pazhouhanfar, Yaghoub [3 ]
Delbari, Seyed Ali [4 ]
Quyet Van Le [5 ]
Shaddel, Shahrzad [6 ]
Pazhouhanfar, Morteza [3 ]
Namini, Abbas Sabahi [7 ,8 ]
Shokouhimehr, Mohammadreza [4 ]
Asl, Mehdi Shahedi [9 ]
机构
[1] Ton Duc Thang Univ, Adv Inst Mat Sci, Lab Adv Mat Chem, Ho Chi Minh City, Vietnam
[2] Ton Duc Thang Univ, Fac Appl Sci, Ho Chi Minh City, Vietnam
[3] Aliyazh Sanat Sahand Ipak Co, POB 51576-13536, Tabriz, Iran
[4] Seoul Natl Univ, Res Inst Adv Mat, Dept Mat Sci & Engn, Seoul 08826, South Korea
[5] Duy Tan Univ, Inst Res & Dev, Da Nang 550000, Vietnam
[6] Sahand Univ Technol, Dept Mat Engn, Tabriz, Iran
[7] Univ Mohaghegh Ardabili, Fac Adv Technol, Dept Engn Sci, Namin, Iran
[8] Sabalan Univ Adv Technol SUAT, Fac Adv Technol, Dept Engn Sci, Namin, Iran
[9] Univ Mohaghegh Ardabili, Dept Mech Engn, Ardebil, Iran
关键词
TiC; Graphene; Characterization; SPS; Ceramic; THERMAL-SHOCK RESISTANCE; HOT-PRESSING PARAMETERS; MECHANICAL-PROPERTIES; MICROSTRUCTURAL DEVELOPMENT; COMPOSITES; SINTERABILITY; DENSIFICATION; TEMPERATURE; SEPARATION; ZRB2;
D O I
10.1016/j.ceramint.2020.04.189
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
This research aims to scrutinize the impact of graphene additive on the consolidation behavior, microstructure and physical-mechanical qualifications of TiC-based materials. For this purpose, two specimens, namely monolithic TiC and TiC-5 wt% graphene, were produced using the spark plasma sintering (SPS) method at 1900 degrees C. An external pressure of 40 MPa was applied during the sintering, and the ceramics were held at the maximum temperature for 10 min. The characteristics of SPSed samples were studied using scanning electron microscopy (SEM) and X-ray diffraction (XRD). Although adding graphene had no notable effect on the sinterability of TiC, it led to an increment in the flexural strength of graphene-doped sample. The microstructural assessment revealed the positive influence of graphene additive on obtaining a finer microstructure. The phase analysis confirmed the appearance of a non-stoichiometric hexagonal TiCx and different allotropes of carbon in the samples. Finally, the highest values for Vickers hardness (similar to 3130 HV0.1Kg) and flexural strength (similar to 530 MPa) were attained for the monolithic TiC and graphene-reinforced samples, respectively.
引用
收藏
页码:18742 / 18749
页数:8
相关论文
共 50 条
  • [31] Properties of TiC and TiN Reinforced Alumina-Zirconia Composites Sintered with Spark Plasma Technique
    Szutkowska, Magdalena
    Cygan, Slawomir
    Podsiadlo, Marcin
    Laszkiewicz-Lukasik, Jolanta
    Cyboron, Jolanta
    Kalinka, Andrzej
    [J]. METALS, 2019, 9 (11)
  • [32] Preparation and characterization of graphene nano-platelets integrated polyaniline based conducting nanocomposites
    Tokala, Mamata Reddy
    Padya, Balaji
    Jain, P. K.
    Chakra, C. H. Shilpa
    [J]. SUPERLATTICES AND MICROSTRUCTURES, 2015, 82 : 287 - 292
  • [33] Effect of solid solution formation on densification of spark plasma sintered ZrC ceramics with TiC as sintering aid
    Niu, B.
    Zhang, F.
    Ji, W.
    Zhang, J. Y.
    Fu, Z. Y.
    Wang, W. M.
    [J]. ADVANCES IN APPLIED CERAMICS, 2016, 115 (01) : 55 - 59
  • [34] EVALUATION OF THE MECHANICAL AND ELECTRICAL PROPERTIES OF SPARK PLASMA SINTERED TITANIUM CARBIDE REINFORCED ALUMINA CERAMIC COMPOSITE
    Selvakumar, G.
    Prakash, S. Ram
    Rajkumar, K.
    [J]. ARCHIVES OF METALLURGY AND MATERIALS, 2021, 66 (03) : 831 - 838
  • [35] Spray deposition of graphene nano-platelets for modifying interleaves in carbon fibre reinforced polymer laminates
    Nagi, Chirnjeev S.
    Ogin, Stephen L.
    Mohagheghian, Iman
    Crean, Carol
    Foreman, Andrew D.
    [J]. MATERIALS & DESIGN, 2020, 193
  • [36] Optical spectroscopy, thermal analysis, and dynamic mechanical properties of graphene nano-platelets reinforced polyvinylchloride
    Ahmed, R. M.
    Atta, M. M.
    Taha, E. O.
    [J]. JOURNAL OF MATERIALS SCIENCE-MATERIALS IN ELECTRONICS, 2021, 32 (17) : 22699 - 22717
  • [37] Improving tribological performance of chemically bonded phosphate ceramic coatings reinforced by graphene nano-platelets
    Bian, Da
    Aradhyula, Thirumala Vasu
    Guo, Yongxin
    Zhao, Yongwu
    [J]. CERAMICS INTERNATIONAL, 2017, 43 (15) : 12466 - 12471
  • [38] Fabrication and Characterization of Polyetherimide Electrospun Scaffolds Modified with Graphene Nano-Platelets and Hydroxyapatite Nano-Particles
    Kostopoulos, Vassilis
    Kotrotsos, Athanasios
    Fouriki, Kalliopi
    Kalarakis, Alexandros
    Portan, Diana
    [J]. INTERNATIONAL JOURNAL OF MOLECULAR SCIENCES, 2020, 21 (02)
  • [39] Densification of nanocrystalline TiC ceramics by spark plasma sintering
    Chaim, Rachman
    Kleiner, Liliya
    Kalabukhov, Sergey
    [J]. MATERIALS CHEMISTRY AND PHYSICS, 2011, 130 (1-2) : 815 - 821
  • [40] Processing and characterization of spark plasma sintered TZM alloy
    Danisman, Can Burak
    Yavas, Baris
    Yucel, Onuralp
    Sahin, Filiz
    Goller, Gultekin
    [J]. JOURNAL OF ALLOYS AND COMPOUNDS, 2016, 685 : 860 - 868