N-(7-Ethoxy-1H-indazol-4-yl)-4-methylbenzenesulfonamide

被引:5
作者
Abbassi, Najat [1 ]
Rakib, El Mostapha [1 ]
Zouihri, Hafid [2 ]
机构
[1] Univ Sultan Moulay Slimane, Lab Chim Organ & Analyt, Fac Sci & Tech, Beni Mellal, Morocco
[2] Ctr Natl Rech Sci & Tech, Lab Diffract Rayons X, Rabat, Morocco
来源
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2011年 / 67卷
关键词
D O I
10.1107/S1600536811016576
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
The molecule of the title heterocyclic compound, C16H17N3O3S, is bent at the S atom with an C-SO2-NH-C torsion angle of 80.17 (8)degrees. The phenyl substituent at the S atom is rotated out of the plane of the 1H-indazole ring [interplanar angle = 46.24 (8)degrees]. In the crystal, intermolecular N-H...N and N-H...O hydrogen bonds build up a ribbon developing parallel to the b-axis direction. C-H...O hydrogen bonds link these ribbons, forming a layer parallel to the bc plane.
引用
收藏
页码:O1354 / U191
页数:10
相关论文
共 10 条
[1]  
[Anonymous], 2005, APEX2 SAINT
[2]   4-Chloro-N-(3-chlorophenyl)-2-methylbenzenesulfonamide [J].
Gowda, B. Thimme ;
Foro, Sabine ;
Nirmala, P. G. ;
Fuess, Hartmut .
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 :O1702-U558
[3]   N-Benzyl-N-ethyl-4-methylbenzenesulfonamide [J].
Khan, Islam Ullah ;
Ahmad, Waqar ;
Arshad, Muhammad Nadeem ;
Sharif, Shahzad ;
Ahmed, Jamil .
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 :O2507-U1892
[4]  
Lee JS, 2002, B KOR CHEM SOC, V23, P167
[5]   Toward the control of Leptosphaeria maculans:: Design, syntheses, biological activity, and metabolism of potential detoxification inhibitors of the crucifer phytoalexin brassinin [J].
Pedras, M. Soledade C. ;
Jha, Mukund .
BIOORGANIC & MEDICINAL CHEMISTRY, 2006, 14 (14) :4958-4979
[6]   N-(2,6-Dichlorophenyl)-4-methylbenzenesulfonamide [J].
Shakuntala, K. ;
Foro, Sabine ;
Gowda, B. Thimme .
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 :O142-U2606
[7]   N-(3,4-Dichlorophenyl)-4-methylbenzenesulfonamide [J].
Shakuntala, K. ;
Foro, Sabine ;
Gowda, B. Thimme .
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 :O104-U2255
[8]   A short history of SHELX [J].
Sheldrick, George M. .
ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2008, 64 :112-122
[9]   Structure validation in chemical crystallography [J].
Spek, Anthony L. .
ACTA CRYSTALLOGRAPHICA SECTION D-STRUCTURAL BIOLOGY, 2009, 65 :148-155
[10]   publCIF: software for editing, validating and formatting crystallographic information files [J].
Westrip, Simon P. .
JOURNAL OF APPLIED CRYSTALLOGRAPHY, 2010, 43 :920-925