One-step conversion of aldehydes into nitriles in dry media under microwave irradiation

被引：24

作者：

Feng, JC ^{[1
]}

Liu, B ^{[1
]}

Dai, L ^{[1
]}

Bian, NS ^{[1
]}

机构：

[1] Nanjing Univ, Dept Chem, Nanjing 210093, Peoples R China

来源：

SYNTHETIC COMMUNICATIONS | 1998年 / 28卷 / 20期

关键词：

D O I：

10.1080/00397919808004928

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

Aldehydes undergo rapid reaction with hydroxylammonium chloride using HCOOH/SiO2 as solid support catalyst, under microwave irradiation without solvent to affords nitriles in 60-90% yields.

引用

页码：3765 / 3768

页数：4

共 11 条

[1]

CAPDEVIELLE P, 1989, SYNTHESIS-STUTTGART, P451

[2]

Feng JC, 1996, SYNTHETIC COMMUN, V26, P4545

[3]

FIZET C, 1974, TETRAHEDRON LETT, P3187

[4]

KARMARKAR SN, 1985, SYNTHESIS-STUTTGART, P510

[5] Microwave promoted rapid dehydration of aldoximes to nitriles on a solid support [J].

Kumar, HMS ;

Mohanty, PK ;

Kumar, MS ;

Yadav, JS .

SYNTHETIC COMMUNICATIONS, 1997, 27 (08) :1327-1333

[6] CONVENIENT, HIGH-YIELD CONVERSION OF ALDEHYDES TO NITRILES [J].

MILLER, MJ ;

LOUDON, GM .

JOURNAL OF ORGANIC CHEMISTRY, 1975, 40 (01) :126-127

[7]

OLAH GA, 1979, SYNTHESIS-STUTTGART, P112

[8]

SOSNOVSKY G, 1907, SYNTHESIS-STUTTGART, P703

[9]

VANES T, 1965, J CHEM SOC, P1564

[10]

VILLEMIN D, 1991, CHEM IND-LONDON, P176

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