Investigation of MAO Coatings Characteristics on Titanium Products Obtained by EBM Method Using Additive Manufacturing

被引:11
作者
Grigoriev, Sergey [1 ]
Peretyagin, Nikita [1 ,2 ]
Apelfeld, Andrey [3 ]
Smirnov, Anton [1 ]
Yanushevich, Oleg [2 ]
Krikheli, Natella [2 ]
Kramar, Olga [2 ]
Kramar, Sergey [2 ]
Peretyagin, Pavel [1 ,2 ]
机构
[1] Moscow State Univ Technol STANKIN, Spark Plasma Sintering Res Lab, Vadkovsky Per 1, Moscow 127055, Russia
[2] AI Evdokimov Moscow State Univ Med & Dent, Dept Sci, Delegatskaya St 20,Build 1, Moscow 127473, Russia
[3] Natl Res Univ, Dept 1203, Moscow Aviat Inst, Volokolamskoe Shosse 4, Moscow 125993, Russia
基金
俄罗斯科学基金会;
关键词
titanium alloy Ti-6Al-4V; additive manufacturing; electron beam melting; micro-arc oxidation; MAO coating; thickness; roughness; surface morphology; structure; composition; heat resistance; thermal cycling test; MICROARC OXIDATION; POROUS TITANIUM; MICROSTRUCTURE; ALLOY; CORROSION; ELECTROLYTES; PERFORMANCE; BEHAVIOR;
D O I
10.3390/ma15134535
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
Coatings with a thickness from 27 to 62 mu m on electron beam melted Ti-6Al-4V have been formed by micro-arc oxidation (MAO) in a silicate-hypophosphite electrolyte. MAO tests in the anode-cathode mode (50 Hz) with an anode-to-cathode current ratio of 1:1 and sum current densities 10 and 20 A/dm(2) were carried out. The duration of the MAO treatment was 30 and 60 min. The effect of the processing parameters on the structural properties of the MAO treated coatings was studied. The current density and treatment time significantly affect the coating thickness and surface roughness. The values of these characteristics increase as the current density increases. The effect of thermal cycling tests on surface morphology, thickness and roughness, and elemental and phase composition of MAO coatings was analyzed. After 50 cycles of thermal cycling from +200 degrees C to -50 degrees C, no cracking or delamination of coatings was observed. Coatings formed in 30 min at a current density of 20 A/dm(2) turned out to be the best in terms of such indicators as surface morphology, thickness, and roughness.
引用
收藏
页数:11
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