C/C-SiC composite fabricated via PCS-Si slurry reactive melt infiltration

被引:8
作者
Guo, Wenjian [1 ]
Bai, Shuxin [1 ]
Ye, Yicong [1 ]
Zhu, Lian [1 ]
Li, Shun [1 ]
机构
[1] Natl Univ Def Technol, Dept Mat Sci & Engn, Coll Aerosp Sci, Changsha 410073, Hunan, Peoples R China
关键词
ablation; C/C-SiC; reactive melt infiltration; slurry; ABLATION BEHAVIOR; SILICON-CARBIDE; LIQUID SILICON; MICROSTRUCTURE; MECHANISM;
D O I
10.1111/ijac.13050
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
The slurry reactive melt infiltration (RMI) method was used to overcome the shortcomings of the traditional RMI method utilized in preparing the large-irregular shaped C/C preform. C/C-SiC composite was successfully fabricated via PCS-Si slurry RMI. Results show that it has a favorable physical bonding between the PCS-Si slurry and the C/C preform. After RMI, most of the Si in the PCS-Si slurry coating infiltrated into the C/C preform, the density of the C/C preform increased from 1.24 to 1.52g cm(-3), and the open porosity decreased from 27.22% to 18.04%. SiC was formed on the surface as well as in the pores of the C/C preform. The as-received C/C-SiC composite showed a pseudo-ductile fracture behavior with a flexural strength of 76.4MPa. The mass ablation rate of the C/C-SiC composite is 0.34 mg s(-1), exhibiting much better ablation resistance than the C/C preform with a mass ablation rate of 1.80 mg s(-1).
引用
收藏
页码:88 / 96
页数:9
相关论文
共 25 条
[1]   Advanced ceramic materials for high temperature applications [J].
Belmonte, Manuel .
ADVANCED ENGINEERING MATERIALS, 2006, 8 (08) :693-703
[2]   Effects of high-temperature annealing on the microstructure and properties of C/ZrC composites prepared by reactive melt infiltration [J].
Chen, Si'an ;
Ji, Hongliang ;
Li, Yong ;
Li, Guangde ;
Mei, Min ;
Hu, Haifeng .
MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING, 2017, 686 :41-45
[3]   Microstructure and properties of ablative C/ZrC-SiC composites prepared by reactive melt infiltration of zirconium and vapour silicon infiltration [J].
Chen, Si'an ;
Li, Guangde ;
Hu, Haifeng ;
Li, Yong ;
Mei, Min .
CERAMICS INTERNATIONAL, 2017, 43 (03) :3439-3442
[4]   3D Cf/SiC-ZrC-ZrB2 composites fabricated via sol-gel process combined with reactive melt infiltration [J].
Chen, Xiaowu ;
Dong, Shaoming ;
Kan, Yanmei ;
Zhou, Haijun ;
Hu, Jianbao ;
Wang, Dengke .
JOURNAL OF THE EUROPEAN CERAMIC SOCIETY, 2016, 36 (15) :3607-3613
[5]   Analysis and characterization of polycarbosilane [J].
Cheng, Xiangzhen ;
Xie, Zhengfang ;
Song, Yongcai ;
Xiao, Jiayu ;
Wang, Yingde .
INTERNATIONAL JOURNAL OF POLYMER ANALYSIS AND CHARACTERIZATION, 2006, 11 (04) :287-298
[6]   Comparative ablation behaviors of C/SiC-HfC composites prepared by reactive melt infiltration and precursor infiltration and pyrolysis routes [J].
Duan, Liuyang ;
Zhao, Xing ;
Wang, Yiguang .
CERAMICS INTERNATIONAL, 2017, 43 (18) :16114-16120
[7]   Analysis of reactive melt infiltration in the processing of ceramics and ceramic composites [J].
Einset, EO .
CHEMICAL ENGINEERING SCIENCE, 1998, 53 (05) :1027-1039
[8]   Synthesis of Ti3SiC2-based materials by reactive melt infiltration [J].
Fan, Xiaomeng ;
Yin, Xiaowei ;
Wang, Lei ;
Greil, Peter ;
Travitzky, Nahum .
INTERNATIONAL JOURNAL OF REFRACTORY METALS & HARD MATERIALS, 2014, 45 :1-7
[9]  
HASEGAWA Y, 1989, J MATER SCI, V24, P1177, DOI 10.1007/BF02397045
[10]   ZrO2-SiO2 gradient multilayer oxidation protective coating for SiC coated carbon/carbon composites [J].
Huang, HF ;
Zeng, XR ;
Li, HJ ;
Xiong, XB ;
Sun, GL .
SURFACE & COATINGS TECHNOLOGY, 2005, 190 (2-3) :255-259