Direct one-step synthesis of mesoporous ZnO-silicate matrix using a true liquid crystal method

被引：2
作者：
Aqeel, Tariq [1 ]
Abdullah, Haifaa N. [2 ]
机构：
[1] Publ Author Appl Educ & Training PAAET Kuwait, Coll Basic Educ, Dept Sci, Safat, Kuwait
[2] PAAET Kuwait, Coll Technol Studies, Dept Labs Appl Chem, Safat, Kuwait
来源：
MAIN GROUP CHEMISTRY | 2018年 / 17卷 / 03期
关键词：
True liquid crystal templating (TLCT); mesoporous ZnO/SiO2 matrix; XPS; EDS; TEM; UV/Vis; THIN-FILMS; ZINC-OXIDE; COLLOIDAL SUSPENSIONS; PARTICLE-SIZE; DEPOSITION; GROWTH; NANOPARTICLES; TEMPERATURE; NANOWIRES; KINETICS;
D O I：
10.3233/MGC-180266
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
In the quest of preparing mesoporous zinc oxide via true liquid crystal templating (TLCT) a novel one-step synthesis was discovered to form a mesoporous zinc oxide/silica matrix using a modified (TLCT) method. 6% wt/wt of ZnO/SiO2 mesoporous structure was successfully synthesized and shown to have the highest BET surface area of 530 m(2) g(-1) reported and pore diameter range of 22-36 angstrom. Transmission Electron Microscopy (TEM), X-ray diffraction (XRD), N-2 sorption analysis, Energy Dispersive X-ray Spectroscopy (EDX/EDS), Scanning Electron Microscopy (SEM) X-ray photoelectron spectrometry (XPS) and Ultraviolet/Visible spectroscopy (UV/VIS) were used to investigate the structural morphology and composition.
引用
收藏
页码：235 / 246
页数：12
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