Orientations of Y2BaCuO5 and YBCO within melt-textured and directional solidified samples studied by EBSD

被引:5
作者
Koblischka, MR
Koblischka-Veneva, A
Reddy, ES
Schmitz, GJ
Ogasawara, K
Murakami, M
机构
[1] Univ Saarland, Inst Expt Phys, D-66041 Saarbrucken, Germany
[2] Univ Saarland, Inst Funct Mat, D-66041 Saarbrucken, Germany
[3] ACCESS eV, Mat & Proc, D-52072 Aachen, Germany
[4] ISTEC, Superconduct Res Lab, Div 3, Minato Ku, Tokyo 1050023, Japan
来源
PHYSICA C-SUPERCONDUCTIVITY AND ITS APPLICATIONS | 2003年 / 392卷
关键词
electron backscatter diffraction; SEM; ceramics; bulk high-T-c superconductors; automated mapping;
D O I
10.1016/S0921-4534(03)00754-8
中图分类号
O59 [应用物理学];
学科分类号
摘要
By means of automated electron backscatter diffraction (EBSD) analysis, we studied the local orientations of embedded Y2BaCuO5 (2 1 1) particles within melt-textured YBCO samples, and also the orientations of embedded YBCO particles in directional solidified 211 samples. On both systems, we obtained high-quality Kikuchi patterns, allowing the automated mapping of the crystal orientations and a multi-phase analysis. In melt-textured YBCO with (00 1) orientation, we find that the embedded 211 particles do not have any preferred orientation, but the maps also reveal that at certain orientations of the 211 particles the YBCO growth is not altered. In directional solidified 211 samples, where the 211 is mainly oriented in (0 0 1) direction, the embedded YBCO particles show only some specific orientations. (C) 2003 Elsevier B.V. All rights reserved.
引用
收藏
页码:589 / 595
页数:7
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