High-throughput characterization of heterogeneous catalysts by temperature-programmed analysis method

被引：18

作者：

Wang, H ^{[1
]}

Liu, ZM ^{[1
]}

Shen, JH ^{[1
]}

Liu, HC ^{[1
]}

机构：

[1] Chinese Acad Sci, Dalian Inst Chem Phys, Nat Gas Utilizat & Appl Catalysis Lab, Dalian 116023, Peoples R China

来源：

CATALYSIS COMMUNICATIONS | 2004年 / 5卷 / 01期

关键词：

D O I：

10.1016/j.catcom.2003.11.001

中图分类号：

O64 [物理化学（理论化学）、化学物理学];

学科分类号：

070304 ; 081704 ;

摘要：

A multistream reactor for high-throughput examining the surface acidity by NH3-TPD method by application of multistream mass spectrometer screening (MSMSS) technique has been developed. This method allows for examining the surface acidity of 10 catalyst samples in about 6 h, which is an improvement over the traditional process. The demonstration of the feasibility of high-throughput TPD can be significant in convincing the hardened traditionalists in the heterogeneous catalysis community that, combinatorial methods indeed should have an important place in scientific catalyst research and development. The developed method could also be used for almost all the temperature-programmed analysis theoretically with careful designed multistream reactors. (C) 2003 Elsevier B.V. All rights reserved.

引用

页码：55 / 58

页数：4

共 28 条

[1] Miniaturization of screening devices for the combinatorial development of heterogeneous catalysts [J].