LC with Electrochemical Detection for Analysis of Caffeic Acid and Caffeic Acid Phenyl Ester in Propolis

被引：16
作者：
Cao, Wei [1 ,2 ]
Liu, Hai-Feng [1 ]
Cheng, Ni [2 ]
Gao, Hui [2 ]
Wang, Bi-Ni [2 ]
Zheng, Jin-Bin [1 ]
机构：
[1] Northwest Univ, Inst Analyt Sci, Shaanxi Prov Key Lab Electroanal Chem, Xian 710069, Shaanxi, Peoples R China
[2] Northwest Univ, Dept Food Sci & Engn, Xian 710069, Shaanxi, Peoples R China
来源：
CHROMATOGRAPHIA | 2011年 / 73卷 / 3-4期
关键词：
Column liquid chromatography; Electrochemical detection; Propolis; Caffeic acid; Caffeic acid phenyl ester; PHENETHYL ESTER; REPERFUSION INJURY; ALPHA-TOCOPHEROL;
D O I：
10.1007/s10337-010-1864-7
中图分类号：
Q5 [生物化学];
学科分类号：
071010 ; 081704 ;
摘要：
A simple, sensitive, and accurate liquid chromatographic method with electrochemical detection (ECD) has been developed for analysis of caffeic acid and caffeic acid phenyl ester in propolis. ECD is more sensitive than diode-array detection for analysis of the two phenolic compounds. The calibration plots show linearity is good (r a parts per thousand yen 0.9995) in the ranges tested. Recovery was from 93.5 to 97.4%.
引用
收藏
页码：411 / 414
页数：4
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