Structural improvement of CVD multi-walled carbon nanotubes by a rapid annealing process

被引：24

作者：

Zhao, Jiang ^{[1
]}

Zhang, Yaozhong ^{[1
]}

Su, Yanjie ^{[1
]}

Huang, Xiaolu ^{[1
]}

Wei, Liangming ^{[1
]}

Kong, Eric Siu-Wai ^{[1
]}

Zhang, Yafei ^{[1
]}

机构：

[1] Shanghai Jiao Tong Univ, Key Lab Thin Films & Microfabricat, Minist Educ, Res Inst Micro Nano Sci & Technol, Shanghai 200240, Peoples R China

来源：

基金：

中国国家自然科学基金; 上海市自然科学基金;

关键词：

Structural improvement; CVD carbon nanotubes; Rapid annealing; Structural analysis; RAMAN-SPECTROSCOPY; PURIFICATION; OXIDATION; BATTERIES;

D O I：

10.1016/j.diamond.2012.01.029

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

Generally, due to structural disorders in multi-walled carbon nanotubes (MWCNTs) synthesized by chemical vapor deposition (CVD), most of their properties are much below the expected values. A novel technique has been developed in this investigation for structural improvement of CVD MWCNTs using a rapid annealing process. Direct observation by transmission electron microscope (TEM) indicates obvious structural changes in the nanotubes after a rapid annealing process between 2000 degrees C and 2800 degrees C, while nanotubes with twisty shells and kinked walls have been observed as the annealing temperature approaches 3000 degrees C. Decrease of I-D/I-G ratio in Raman spectra, increase of the starting oxidation temperature observed in Thermogravimetric analysis (TGA), as well as increase in electrical conductivity of nanotube powders suggests the reconstruction toward more ordered nanotube structure after a rapid high temperature annealing process. (C) 2012 Elsevier B.V. All rights reserved.

引用

页码：24 / 28

页数：5

共 50 条

[1] Rapid Structural Improvement of CVD-Grown Multi-Walled Carbon Nanotubes by Drastic Thermite Reaction
Zhao, Jiang
Chen, Jing
Zhang, Pengcheng
Yu, Haofeng
Chen, Jie
NANO, 2015, 10 (08)
[2] Characterisation of commercially CVD grown multi-walled carbon nanotubes for paint applications
White, Christopher M.
Banks, Richard
Hamerton, Ian
Watts, John F.
PROGRESS IN ORGANIC COATINGS, 2016, 90 : 44 - 53
[3] Defect Reduction of Multi-walled Carbon Nanotubes by Rapid Vacuum Arc Annealing
Tsai, Jeff T. H.
Li, Jason S.
Tseng, Anders A. P.
NSTI NANOTECH 2008, VOL 1, TECHNICAL PROCEEDINGS: MATERIALS, FABRICATION, PARTICLES, AND CHARACTERIZATION, 2008, : 122 - +
[4] Raman spectra for characterization of defective CVD multi-walled carbon nanotubes
Kuznetsov, Vladimir L.
Bokova-Sirosh, Sofya N.
Moseenkov, Sergey I.
Ishchenko, Arcady V.
Krasnikov, Dmitry V.
Kazakova, Mariya A.
Romanenko, Anatoly I.
Tkachev, Evgeniy N.
Obraztsova, Elena D.
PHYSICA STATUS SOLIDI B-BASIC SOLID STATE PHYSICS, 2014, 251 (12): : 2444 - 2450
[5] Defect-dependent annealing behavior of multi-walled carbon nanotubes
Bhalerao, G. M.
Sinha, A. K.
Sathe, V.
PHYSICA E-LOW-DIMENSIONAL SYSTEMS & NANOSTRUCTURES, 2008, 41 (01) : 54 - 59
[6] The oxidation kinetics of multi-walled carbon nanotubes
Singh, Ankit Kumar
Hou, Xin-mei
Chou, Kuo-Chih
CORROSION SCIENCE, 2010, 52 (05) : 1771 - 1776
[7] Purification of multi-walled carbon nanotubes
Li, QL
Yuan, DX
Lin, QM
ACTA CHIMICA SINICA, 2003, 61 (06) : 931 - 936
[8] Preparation and characterization of hydroxylated multi-walled carbon nanotubes
Ling, Xin-Long
Wei, Yi-Zhe
Zou, Li-Ming
Xu, Su
COLLOIDS AND SURFACES A-PHYSICOCHEMICAL AND ENGINEERING ASPECTS, 2013, 421 : 9 - 15
[9] Pulsed laser heating process of multi-walled carbon nanotubes film
Nakamiya, Toshiyuki
Ueda, Tsuyoshi
Ikegami, Tomoaki
Mitsugi, Fumiaki
Ebihara, Kenji
Tsuda, Ryoichi
DIAMOND AND RELATED MATERIALS, 2008, 17 (7-10) : 1458 - 1461
[10] Pristine Multi-walled carbon nanotubes for a rapid and efficient plasmid DNA clarification
Ferreira, P.
Riscado, M.
Bernardo, S.
Freire, M. G.
Faria, J. L.
Tavares, APM.
Silva, CG.
Sousa, F.
SEPARATION AND PURIFICATION TECHNOLOGY, 2023, 320

← 1 2 3 4 5 →