Electrochemical synthesis of spiroisoxazole derivatives and its application to natural products

被引:0
作者
Ogamino, T [1 ]
Ishikawa, Y [1 ]
Nishiyama, S [1 ]
机构
[1] Keio Univ, Fac Sci & Technol, Dept Chem, Kohoku Ku, Yokohama, Kanagawa 2238522, Japan
关键词
spiroisoxazole; anodic oxidation; zamamistatin; dibromophenylpyruvic acid oxime; phenolic oxidation;
D O I
暂无
中图分类号
O62 [有机化学];
学科分类号
070303 ; 081704 ;
摘要
Efficient synthesis of the trans-spiroisoxazole (1) and its unnatural cis-isomer (2) was accomplished by employing anodic oxidation of 4, followed by Zn(BH4)(2) reduction. This method was applied to an assembly of the carbon framework of zamamistatin (12).
引用
收藏
页码:73 / +
页数:7
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