Densification behavior and microstructure of spark plasma sintered ZrB2-based composites with SiC particles

被引：47

作者：

Ikegami, Masahide ^{[2
]}

Guo, Shuqi ^{[1
]}

Kagawa, Yutaka ^{[1
,2
]}

机构：

[1] Natl Inst Mat Sci, Hybrid Mat Unit, Tsukuba, Ibaraki 3050047, Japan

[2] Univ Tokyo, Res Ctr Adv Sci & Technol, Meguro Ku, Tokyo 1538505, Japan

来源：

CERAMICS INTERNATIONAL | 2012年 / 38卷 / 01期

关键词：

ZrB2; Densification; Microstructure; Spark plasma sintering; HIGH-TEMPERATURE CERAMICS; MECHANICAL-PROPERTIES; PHYSICAL-PROPERTIES; OXIDATION; ZRB2;

D O I：

10.1016/j.ceramint.2011.08.003

中图分类号：

TQ174 [陶瓷工业]; TB3 [工程材料学];

学科分类号：

0805 ; 080502 ;

摘要：

The densification behavior and microstructure of spark plasma sintered ZrB2-based composites with SiC particles were examined. The effects of the amount and size of the SIC particles added were assessed. The results indicated that sinterability of the composites was improved by the addition of SiC compared with single-phase ZrB2 ceramics. This improvement depended on the effects of the amount and size of SIC particles added. Relative densities exceeding 98% were obtained for ZrB2-SiC powders sintered at 1900 degrees C for 2 min under a pressure of 30 MPa. The microstructure of the resulting composites was fine and homogeneous, and the average grain size of ZrB2 decreased with increase in the amount of SiC and with decrease in SiC particle size. (C) 2011 Elsevier Ltd and Techna Group S.r.l. All rights reserved.

引用

页码：769 / 774

页数：6

共 23 条

[1] Synthesis and characterization of dense ultra-high temperature thermal protection materials produced by field activation through spark plasma sintering (SPS): I. Hafnium Diboride [J].

Anselmi-Tamburini, U ;

Kodera, Y ;

Gasch, M ;

Unuvar, C ;

Munir, ZA ;

Ohyanagi, M ;

Johnson, SM .

JOURNAL OF MATERIALS SCIENCE, 2006, 41 (10) :3097-3104

[2] EFFECT OF OXYGEN CONTAMINATION ON DENSIFICATION OF TIB2 [J].

BAIK, S ;

BECHER, PF .

JOURNAL OF THE AMERICAN CERAMIC SOCIETY, 1987, 70 (08) :527-530

[3] Fast densification of ultra-high-temperature ceramics by spark plasma sintering [J].

Bellosi, A ;

Monteverde, FD ;

Sciti, D .

INTERNATIONAL JOURNAL OF APPLIED CERAMIC TECHNOLOGY, 2006, 3 (01) :32-40

[4] Processing and characterization of ZrB2-based ultra-high temperature monolithic and fibrous monolithic ceramics [J].

Fahrenholtz, WG ;

Hilmas, GE ;

Chamberlain, AL ;

Zimmermann, JW .

JOURNAL OF MATERIALS SCIENCE, 2004, 39 (19) :5951-5957

[5] Effect of thermal exposure on strength of ZrB2-based composites with nano-sized SiC particles [J].

Guo, Shu-Qi ;

Yang, Jenn-Ming ;

Tanaka, Hidehiko ;

Kagawa, Yutaka .

COMPOSITES SCIENCE AND TECHNOLOGY, 2008, 68 (14) :3033-3040

[6] Spark plasma sintering of zirconium diborides [J].

Guo, Shu-Qi ;

Nishimura, Toshiyuki ;

Kagawa, Yutaka ;

Yang, Jenn-Ming .

JOURNAL OF THE AMERICAN CERAMIC SOCIETY, 2008, 91 (09) :2848-2855

[7] Mechanical and physical behavior of spark plasma sintered ZrC-ZrB2-SiC composites [J].

Guo, Shu-Qi ;

Kagawa, Yutaka ;

Nishimura, Toshiyuki ;

Chung, Dowhan ;

Yang, Jenn-Ming .

JOURNAL OF THE EUROPEAN CERAMIC SOCIETY, 2008, 28 (06) :1279-1285

[8] Pressureless sintering and physical properties of ZrB2-based composites with ZrSi2 additive [J].

Guo, Shu-Qi ;

Kagawa, Yutaka ;

Nishimura, Toshiyuki ;

Tanaka, Hidehiko .

SCRIPTA MATERIALIA, 2008, 58 (07) :579-582

[9] Densification of ZrB2-based composites and their mechanical and physical properties: A review [J].

Guo, Shu-Qi .

JOURNAL OF THE EUROPEAN CERAMIC SOCIETY, 2009, 29 (06) :995-1011

[10] Flexural strength and fracture behavior of ZrB2-SiC ultra-high temperature ceramic composites at 1800°C [J].

Hu, Ping ;

Wang, Zhi .

JOURNAL OF THE EUROPEAN CERAMIC SOCIETY, 2010, 30 (04) :1021-1026

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