Electron Diffraction of 3D Molecular Crystals

被引：56

作者：

Saha, Ambarneil ^{[1
,2
]}

Nia, Shervin S. ^{[1
,2
]}

Rodriguez, Jose A. ^{[1
,2
]}

机构：

[1] Univ Calif Los Angeles, UCLA DOE Inst Genom & Prote, Los Angeles, CA 90095 USA

[2] Univ Calif Los Angeles, Dept Chem & Biochem, Los Angeles, CA 90095 USA

来源：

CHEMICAL REVIEWS | 2022年 / 122卷 / 17期

关键词：

ACTIVE PHARMACEUTICAL INGREDIENTS; INITIO STRUCTURE DETERMINATION; STRUCTURE-BASED INHIBITORS; X-RAY CRYSTALLOGRAPHY; RADIATION-DAMAGE; PHASE DETERMINATION; SCATTERING FACTORS; DYNAMICAL DIFFRACTION; PRECESSION TECHNIQUE; HYDROGEN POSITIONS;

D O I：

10.1021/acs.chemrev.1c00879

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

Electron crystallography has a storied history which rivals that of its more established X-ray-enabled counterpart. Recent advances in data collection and analysis have sparked a renaissance in the field, opening a new chapter for this venerable technique. Burgeoning interest in electron crystallography has spawned innovative methods described by various interchangeable labels (3D ED, MicroED, cRED, etc.). This Review covers concepts and findings relevant to the practicing crystallographer, with an emphasis on experiments aimed at using electron diffraction to elucidate the atomic structure of three-dimensional molecular crystals.

引用

页码：13883 / 13914

页数：32

共 289 条

[1] Joint X-ray and neutron refinement with phenix.refine [J].

Afonine, Pavel V. ;

Mustyakimov, Marat ;

Grosse-Kunstleve, Ralf W. ;

Moriarty, Nigel W. ;

Langan, Paul ;

Adams, Paul D. .

ACTA CRYSTALLOGRAPHICA SECTION D-STRUCTURAL BIOLOGY, 2010, 66 :1153-1163

[2] TRIPLET AND QUARTET RELATIONSHIPS AND THE POSITIVITY POSTULATE [J].

ALTOMARE, A ;

GIACOVAZZO, C ;

GUAGLIARDI, A ;

SILIQI, D .

ACTA CRYSTALLOGRAPHICA SECTION A, 1994, 50 :311-317

[3] Waterworks-specific composition of drinking water disinfection by-products [J].

Andersson, Anna ;

Harir, Mourad ;

Gonsior, Michael ;

Hertkorn, Norbert ;

Schmitt-Kopplin, Philippe ;

Kylin, Henrik ;

Karlsson, Susanne ;

Ashiq, Muhammad Jamshaid ;

Lavonen, Elin ;

Nilsson, Kerstin ;

Pettersson, AEmma ;

Stavklint, Helena ;

Bastviken, David .

ENVIRONMENTAL SCIENCE-WATER RESEARCH & TECHNOLOGY, 2019, 5 (05) :861-872

[4] A new olanzapine cocrystal obtained from volatile deep eutectic solvents and determined by 3D electron diffraction [J].

Andrusenko, Iryna ;

Potticary, Jason ;

Hall, Simon R. ;

Gemmi, Mauro .

ACTA CRYSTALLOGRAPHICA SECTION B-STRUCTURAL SCIENCE CRYSTAL ENGINEERING AND MATERIALS, 2020, 76 :1036-1044

[5] The Crystal Structure of Orthocetamol Solved by 3D Electron Diffraction [J].

Andrusenko, Iryna ;

Hamilton, Victoria ;

Mugnaioli, Enrico ;

Lanza, Arianna ;

Hall, Charlie ;

Potticary, Jason ;

Hall, Simon R. ;

Gemmi, Mauro .

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION, 2019, 58 (32) :10919-10922

[6]

[Anonymous], 2022, CAMBRIDGE STRUCTURAL, DOI [10.5517/ccdc.csd.cc26m422, DOI 10.5517/CCDC.CSD.CC26M422]

[7] NBEAM LATTICE IMAGES .3. UPPER LIMITS OF IONICITY IN W4NB26O77 [J].

ANSTIS, GR ;

LYNCH, DF ;

MOODIE, AF ;

OKEEFE, MA .

ACTA CRYSTALLOGRAPHICA SECTION A, 1973, A 29 (MAR1) :138-&

[8] Precession technique and electron diffractometry as new tools for crystal structure analysis and chemical bonding determination [J].

Avilov, A. ;

Kuligin, K. ;

Nicolopoulos, S. ;

Nickolskiy, M. ;

Boulahya, K. ;

Portillo, J. ;

Lepeshov, G. ;

Sobolev, B. ;

Collette, J. P. ;

Martin, N. ;

Robins, A. C. ;

Fischione, P. .

ULTRAMICROSCOPY, 2007, 107 (6-7) :431-444

[9] Accurate prediction of protein structures and interactions using a three-track neural network [J].

Baek, Minkyung ;

DiMaio, Frank ;

Anishchenko, Ivan ;

Dauparas, Justas ;

Ovchinnikov, Sergey ;

Lee, Gyu Rie ;

Wang, Jue ;

Cong, Qian ;

Kinch, Lisa N. ;

Schaeffer, R. Dustin ;

Millan, Claudia ;

Park, Hahnbeom ;

Adams, Carson ;

Glassman, Caleb R. ;

DeGiovanni, Andy ;

Pereira, Jose H. ;

Rodrigues, Andria V. ;

van Dijk, Alberdina A. ;

Ebrecht, Ana C. ;

Opperman, Diederik J. ;

Sagmeister, Theo ;

Buhlheller, Christoph ;

Pavkov-Keller, Tea ;

Rathinaswamy, Manoj K. ;

Dalwadi, Udit ;

Yip, Calvin K. ;

Burke, John E. ;

Garcia, K. Christopher ;

Grishin, Nick V. ;

Adams, Paul D. ;

Read, Randy J. ;

Baker, David .

SCIENCE, 2021, 373 (6557) :871-+

[10] An amyloid-forming peptide from the yeast prion Sup35 reveals a dehydrated β-sheet structure for amyloid [J].

Balbirnie, M ;

Grothe, R ;

Eisenberg, DS .

PROCEEDINGS OF THE NATIONAL ACADEMY OF SCIENCES OF THE UNITED STATES OF AMERICA, 2001, 98 (05) :2375-2380

← 1 2 3 4 5 6 7 8 9 10 →