Fractionation and characterization of nano- and microparticles in liquid media

被引:74
作者
Fedotov, Petr S. [1 ]
Vanifatova, Nataliya G. [1 ]
Shkinev, Valery M. [1 ]
Spivakov, Boris Ya. [1 ]
机构
[1] Russian Acad Sci, Vernadsky Inst Geochem & Analyt Chem, Moscow 119991, Russia
关键词
Nanoparticles; Microparticles; Separation; Characterization; Membrane filtration; Field-flow fractionation; Chromatography; Electrokinetic methods; Hyphenated" techniques; FIELD-FLOW-FRACTIONATION; CAPILLARY-ZONE-ELECTROPHORESIS; SIZE-EXCLUSION CHROMATOGRAPHY; WALLED CARBON NANOTUBES; GRAVITATIONAL SPLITT FRACTIONATION; BORE HYDRODYNAMIC CHROMATOGRAPHY; MONOLAYER-PROTECTED CLUSTERS; IRON-OXIDE NANOPARTICLES; DYNAMIC LIGHT-SCATTERING; VIRUS-LIKE PARTICLES;
D O I
10.1007/s00216-011-4704-1
中图分类号
Q5 [生物化学];
学科分类号
071010 ; 081704 ;
摘要
Submicron and micron particles present in liquid environmental, biological, and technological samples differ in their dimensions, shape, mass, chemical composition, and charge. Their properties cannot be reliably studied unless the particles are fractionated. Synthetic particles applied as components of analytical systems may also need preliminary fractionation and investigation. The review is focused on the methods for fractionation and characterization of nanoparticles and microparticles in liquid media, the most representative examples of their application, and the trends in developing novel approaches to the separation and investigation of particles. Among the separation techniques, the main attention is devoted to membrane filtration, field-flow fractionation, chromatographic, and capillary electrokinetic methods. Microfluidic systems employing the above-mentioned and other separation principles and providing a basis for the fabrication of lab-on-chip devices are also examined. Laser light scattering methods and other physical techniques for the characterization of particles are considered. Special attention is given to "hyphenated" techniques which enable the separation and characterization of particles to be performed in online modes.
引用
收藏
页码:1787 / 1804
页数:18
相关论文
共 178 条
[11]   Structure-assigned optical spectra of single-walled carbon nanotubes [J].
Bachilo, SM ;
Strano, MS ;
Kittrell, C ;
Hauge, RH ;
Smalley, RE ;
Weisman, RB .
SCIENCE, 2002, 298 (5602) :2361-2366
[12]   Rapid Separation and Purification of Nanoparticles in Organic Density Gradients [J].
Bai, Lu ;
Ma, Xiuju ;
Liu, Junfeng ;
Sun, Xiaoming ;
Zhao, Dongyuan ;
Evans, David G. .
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 2010, 132 (07) :2333-2337
[13]   Continuous particle separation in spiral microchannels using dean flows and differential migration [J].
Bhagat, Ali Asgar S. ;
Kuntaegowdanahalli, Sathyakumar S. ;
Papautsky, Ian .
LAB ON A CHIP, 2008, 8 (11) :1906-1914
[14]   On-chip hydrodynamic chromatography separation and detection of nanoparticles and biomolecules [J].
Blom, MT ;
Chmela, E ;
Oosterbroek, RE ;
Tijssen, R ;
van den Berg, A .
ANALYTICAL CHEMISTRY, 2003, 75 (24) :6761-6768
[15]   Metal associations to microparticles, nanocolloids and macromolecules in compost leachates: Size characterization by asymmetrical flow field-flow fractionation coupled to ICP-MS [J].
Bolea, E. ;
Laborda, F. ;
Castillo, J. R. .
ANALYTICA CHIMICA ACTA, 2010, 661 (02) :206-214
[16]   Particle size characterization by quadruple-detector hydrodynamic chromatography [J].
Brewer, Amandaa K. ;
Striegel, Andre M. .
ANALYTICAL AND BIOANALYTICAL CHEMISTRY, 2009, 393 (01) :295-302
[17]   Electrophoretic analysis of gold nanoparticles:: size-dependent electrophoretic mobility of nanoparticles [J].
Buecking, W. ;
Nann, T. .
IEE PROCEEDINGS-NANOBIOTECHNOLOGY, 2006, 153 (03) :47-53
[18]  
Buffle J.v. L., 1993, Environmental Particles
[19]   Effect of ultrasonic treatment on structure and properties of ethylhydroxyethylcellulose polymer adsorption layer on inorganic pigments in aqueous dispersion [J].
Bulychev, N. ;
Dirnberger, K. ;
Arutunov, I. ;
Kopold, P. ;
Schauer, T. ;
Zubov, V. ;
Eisenbach, C. D. .
PROGRESS IN ORGANIC COATINGS, 2008, 62 (03) :299-306
[20]   Particles in natural surface waters: Chemical composition and size distribution [J].
Buykx, SEJ ;
Van den Hoop, MAGT ;
Cleven, RFMJ ;
Buffle, J ;
Wilkinson, KJ .
INTERNATIONAL JOURNAL OF ENVIRONMENTAL ANALYTICAL CHEMISTRY, 2000, 77 (01) :75-93