"Eau de graphene" from a KC8 graphite intercalation compound prepared by a simple mixing of graphite and molten potassium

被引：23

作者：

Bepete, George ^{[1
,2
]}

Hof, Ferdinand ^{[1
,2
]}

Huang, Kai ^{[1
,2
]}

Kampioti, Katerina ^{[1
,2
]}

Anglaret, Eric ^{[3
]}

Drummond, Carlos ^{[1
,2
]}

Penicaud, Alain ^{[1
,2
]}

机构：

[1] CNRS, CRPP, UPR 8641, F-33600 Pessac, France

[2] Univ Bordeaux, CRPP, UPR 8641, F-33600 Pessac, France

[3] Univ Montpellier, Lab Charles Coulomb L2C, CNRS, UMR 5521, F-34000 Montpellier, France

来源：

PHYSICA STATUS SOLIDI-RAPID RESEARCH LETTERS | 2016年 / 10卷 / 12期

关键词：

graphite intercalation compound; KC8; graphenide; eau de graphene; Raman spectroscopy; 2D band; FEW-LAYER GRAPHENE; RAMAN-SPECTROSCOPY; FUNCTIONALIZATION; EXFOLIATION;

D O I：

10.1002/pssr.201600167

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

We synthesized KC8 by simply mixing molten potassium and graphite at 180 degrees C under inert atmosphere. The KC8 shows typical shiny bronze color, Raman characteristics and XRD pattern of an efficiently intercalated stage 1 GIC, and is of sufficient quality to produce fully exfoliated graphenide solutions in tetrahydrofuran (THF) and subsequently single layer graphene in water as "eau de graphene" (EdG). The evolution of absorption and Raman spectroscopic signatures of the EdG as a function of processing conditions give key indications on the number of layers of the graphene flakes dispersed in EdG. (C) 2016 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim

引用

页码：895 / 899

页数：5

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