GO-Fe3O4-Ti(IV) as an efficient magnetic catalyst for the synthesis of bis(indolyl)methanes and benzo[a]xanthen-11-one derivatives

被引:7
作者
Amiri-Zirtol, Leila [1 ]
Amrollahi, Mohammad Ali [1 ]
Mirjalili, Bibi-Fatemeh [1 ]
机构
[1] Yazd Univ, Dept Chem, Yazd, Iran
关键词
Bis(indole)methane; Benzo[a]xanthen-11-one; Heterogeneous Lewis acid; magnetic catalyst; GO-based catalyst; ONE-POT SYNTHESIS; CHROMATOGRAPHY-FREE SYNTHESIS; CROSS-COUPLING REACTION; REUSABLE CATALYST; IONIC LIQUID; FE+3-MONTMORILLONITE K10; REGIOSELECTIVE SYNTHESIS; HETEROGENEOUS CATALYST; HIGHLY EFFICIENT; GREEN SYNTHESIS;
D O I
10.1080/24701556.2021.1980039
中图分类号
O61 [无机化学];
学科分类号
070301 ; 081704 ;
摘要
In this study, a new and efficient magnetic composite was synthesized based on graphene oxide (GO). Initially, GO was coated with magnetite, and then Ti-(IV()) was fixed on GO-Fe3O4 via a covalent graft. The magnetic composite was characterized by FT-IR, EDS, XRD, FE-SEM, TEM, VSM and TGA techniques. It was designed as a compound with strong and recoverable catalytic properties. The prepared GO-Fe3O4-Ti-(IV) emerged to be of high catalytic activity for the synthesis of bis(indolyl)methane and benzo[a]xanthen-11-one derivatives under mild conditions. The stability and reusability of the catalyst were investigated too. All of the data proved that GO-Fe3O4-Ti-(IV) could be recycled five times without a marked loss of activity.
引用
收藏
页码:1211 / 1221
页数:11
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