In situ lift-out: Steps to improve yield and a comparison with other FIB TEM sample preparation techniques

被引:95
作者
Langford, R. M. [1 ]
Rogers, M. [2 ,3 ]
机构
[1] Univ Manchester, Ctr Mat Sci, Manchester M1 7HS, Lancs, England
[2] Graz Univ Technol, Inst Electron Microscopy, A-8010 Graz, Austria
[3] Austriamicrosyst AG, A-8141 Unterpremstatten, Unterpremstatte, Austria
关键词
FIB; In situ lift-out; TEM;
D O I
10.1016/j.micron.2008.02.006
中图分类号
TH742 [显微镜];
学科分类号
摘要
Steps to improve the success yield of the in situ lift-out technique are presented. These include tapping the plinth of the system and monitoring the grounding current to check the lift-out needle is fixed to the material being removed. In addition, the relative success yields and the time to prepare a TEM lamella for the three main FIB methods are discussed and compared. (C) 2008 Elsevier Ltd. All rights reserved.
引用
收藏
页码:1325 / 1330
页数:6
相关论文
共 14 条
[1]  
[Anonymous], 1999, P P 25 INT S TEST FA
[2]  
BASILE DP, 1992, MATER RES SOC SYMP P, V254, P23
[3]  
Bender H, 1999, INST PHYS CONF SER, P593
[4]   Preparation of transmission electron microscope specimens from FeAl and WC powders using focused-ion beam milling [J].
Cairney, JM ;
Munroe, PR .
MATERIALS CHARACTERIZATION, 2001, 46 (04) :297-304
[5]  
KEMPSHALL BW, 2002, ICEM, P249
[6]  
Kirk E. C. G., 1989, Microscopy of Semiconducting Materials 1989. Proceedings of the Royal Microscopical Society Conference, P501
[7]   Focused ion beams techniques for nanomaterials characterization [J].
Langford, Richard M. .
MICROSCOPY RESEARCH AND TECHNIQUE, 2006, 69 (07) :538-549
[8]   Recent advances in FIB-TEM specimen preparation techniques [J].
Li, Jian ;
Malis, T. ;
Dionne, S. .
MATERIALS CHARACTERIZATION, 2006, 57 (01) :64-70
[9]   TEM sample preparation and FIB-induced damage [J].
Mayer, Joachim ;
Giannuzzi, Lucille A. ;
Kamino, Takeo ;
Michael, Joseph .
MRS BULLETIN, 2007, 32 (05) :400-407
[10]   Preparative methods for nanoanalysis of materials with focused ion beam instruments [J].
Nellen, Philipp M. ;
Callegari, Victor ;
Sennhauser, Urs .
CHIMIA, 2006, 60 (11) :A735-A741