Role of material processing on the thermal stability and sinterability of nanocrystalline hydroxyapatite

被引:20
作者
Girija, E. K. [1 ]
Kumar, G. Suresh [1 ]
Thamizhavel, A. [2 ]
Yokogawa, Y. [3 ]
Kalkura, S. Narayana [4 ]
机构
[1] Periyar Univ, Dept Phys, Salem 636011, India
[2] Tata Inst Fundamental Res, Dept Condensed Matter Phys, Bombay 400005, Maharashtra, India
[3] Osaka City Univ, Dept Intelligent Mat Engn, Grad Sch Engn, Osaka 5588585, Japan
[4] Anna Univ, Ctr Crystal Growth, Madras 600025, Tamil Nadu, India
关键词
Hydroxyapatite; Sintering; Thermal stability; Ultrasonication; Freeze drying; WET PRECIPITATION PROCESS; MECHANICAL-PROPERTIES; FLUORIDATED HYDROXYAPATITE; POROUS HYDROXYAPATITE; CERAMICS; NANOPARTICLES; BEHAVIOR;
D O I
10.1016/j.powtec.2012.04.007
中图分类号
TQ [化学工业];
学科分类号
0817 ;
摘要
Hydroxyapatite (HA) resembles natural bone mineral in its major composition and is widely applied for various biomedical applications in different forms. Wet chemical precipitation is an economic and simple route to synthesize HA. But the thermal stability and other related properties of synthesized HA depend on various factors. Here we demonstrate that when ultrasonication is coupled with synthesis and specimen is dried via sublimation (freeze drying) instead of the conventional hot air drying the thermal stability, densification and sinterability are improved. (C) 2012 Elsevier B.V. All rights reserved.
引用
收藏
页码:190 / 195
页数:6
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