Growth, structural, optical and laser damage threshold studies of organic picolinium picrate monohydrate single crystals

被引:9
作者
Pandi, P. [1 ,2 ]
Peramaiyan, G. [1 ]
Bhagavannarayana, G. [3 ]
Kumar, R. Mohan [1 ]
Jayavel, R. [4 ]
机构
[1] Presidency Coll, Dept Phys, Madras 600005, Tamil Nadu, India
[2] Panimalar Engn Coll, Dept Phys, Madras 600123, Tamil Nadu, India
[3] Natl Phys Lab, Mat Characterizat Div, New Delhi 110012, India
[4] Anna Univ, Ctr Crystal Growth, Madras 600025, Tamil Nadu, India
来源
OPTIK | 2013年 / 124卷 / 22期
关键词
Organic compounds; Optical materials; Crystal growth; X-ray diffraction; Mechanical properties; DEFECTS;
D O I
10.1016/j.ijleo.2013.04.058
中图分类号
O43 [光学];
学科分类号
070207 ; 0803 ;
摘要
Picolinium picrate monohydrate (PPM), an organic optical material, was synthesized and single crystals were grown by slow evaporation solution technique. The cell parameters of PPM were confirmed by single crystal X-ray diffraction analysis. The PPM crystals were subjected to FT-IR spectral analyses to confirm the synthesized compound. UV-vis-NIR spectral studies revealed that the optical transparency window of PPM crystal spreads over in the visible and NIR (480-900 nm) regions. From the transmittance data, the optical band gap as function of photon energy was estimated. The microhardness studies were carried out on PPM crystal. The laser damage threshold of PPM crystal was measured using Nd:YAG laser. (C) 2013 Elsevier GmbH. All rights reserved.
引用
收藏
页码:5792 / 5796
页数:5
相关论文
共 18 条
[1]  
[Anonymous], 1987, Nonlinear Optical Properties of Organic a. Molecules and Crystals
[2]   On the electrical and optical properties of CdS films thermally deposited by a modified source [J].
Ashour, A ;
ElKadry, N ;
Mahmoud, SA .
THIN SOLID FILMS, 1995, 269 (1-2) :117-120
[3]   DYNAMICAL DIFFRACTION OF X RAYS BY PERFECT CRYSTALS [J].
BATTERMAN, BW ;
COLE, H .
REVIEWS OF MODERN PHYSICS, 1964, 36 (03) :681-&
[4]   An interesting correlation between crystalline perfection and second harmonic generation efficiency on KCI- and oxalic acid-doped ADP crystals [J].
Bhagavannarayana, G. ;
Parthiban, S. ;
Meenakshisundaram, Subbiah .
CRYSTAL GROWTH & DESIGN, 2008, 8 (02) :446-451
[5]   Interesting growth features in potassium dihydrogen phosphate: unravelling the origin and dynamics of point defects in single crystals [J].
Bhagavannarayana, G. ;
Rajesh, P. ;
Ramasamy, P. .
JOURNAL OF APPLIED CRYSTALLOGRAPHY, 2010, 43 :1372-1376
[6]   Third-order nonlinear optical properties of sulfur-rich compounds [J].
Breitzer, JG ;
Dlott, DD ;
Iwaki, LK ;
Kirkpatrick, SM ;
Rauchfuss, TB .
JOURNAL OF PHYSICAL CHEMISTRY A, 1999, 103 (35) :6930-6937
[7]   Dipole orientation effects on nonlinear optical properties of organic molecular aggregates [J].
Datta, A ;
Pati, SK .
JOURNAL OF CHEMICAL PHYSICS, 2003, 118 (18) :8420-8427
[8]   Influence of strontium doping on the indirect band gap and optical constants of ammonium zinc chloride crystals [J].
Gaffar, MA ;
Abu El-Fadl, A ;
Bin Anooz, S .
PHYSICA B-CONDENSED MATTER, 2003, 327 (01) :43-54
[9]   Influence of postdeposition annealing on the structural and optical properties of sputtered zinc oxide film [J].
Gupta, V ;
Mansingh, A .
JOURNAL OF APPLIED PHYSICS, 1996, 80 (02) :1063-1073
[10]   Study of the influence of dopants on the crystalline perfection of ferroelectric glycine phosphite single crystals using high-resolution X-ray diffraction analysis [J].
Kumar, Krishnamurthy Senthil ;
Babu, Sridharan Moorthy ;
Bhagavannarayana, G. .
JOURNAL OF APPLIED CRYSTALLOGRAPHY, 2011, 44 :313-318