Synthesis of 2-Hydroxy-3-nitro/amino-5-methyl-α-substituted Thiocarbamidoacetophenones

被引:0
作者
Aswale, S. R. [1 ]
Aswale, S. S. [1 ]
Gawhale, N. D. [2 ]
Kodape, M. M. [3 ]
机构
[1] Lokmanya Tilak Mahavidyalaya, Dept Chem, Wani 442304, India
[2] BP Sci Coll, Dept Chem, Digras 445203, India
[3] St Gadge Baba Amravati Univ, Dept Chem, Amravati 444602, India
关键词
2-Hydroxy-3-nitro/amino-5-methyl-alpha-bromoacetophenone; Thioureas; Acetone-ethanol medium; MYCOBACTERIUM-TUBERCULOSIS COMPLEX; ACETOPHENONES; DERIVATIVES; INHIBITION;
D O I
暂无
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
The interactions of 2-hydroxy-3-nitro/amino-5-methyl-alpha-bromoacetophenone (1) with various thioureas (5a-f) in 1:1 molar proportion in acetone-ethanol medium on water bath for 6 h in round bottom flask to synthesis new series of 2-hydroxy-3-nitro/amino-5-methyl-alpha-substituted thiocarbamidoacetophenones (6a-f). The synthesized compounds in these reaction conditions have been characterized on the basis of conventional elemental analysis, chemical characteristic and IR, NMR spectral data.
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页码:5800 / 5802
页数:3
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