Synthesis of Carbon Nanotube Through Sonochemical Process Under Ambient Conditions

被引：11

作者：

Raja, Mohan ^{[1
]}

Ryu, Sung Hun ^{[1
]}

机构：

[1] Kyung Hee Univ, Coll Environm & Appl Chem, Green Energy Ctr, Ind Liaison Res Inst, Yongin 449701, Kyunggi Do, South Korea

来源：

JOURNAL OF NANOSCIENCE AND NANOTECHNOLOGY | 2009年 / 9卷 / 10期

关键词：

Sonochemical Method; ZnCl2; Carbon Nanotubes; Raman Spectroscopy; XRD; HR-TEM; RAMAN-SPECTROSCOPY; GROWTH; TEMPERATURE; ULTRASOUND; ROUTE;

D O I：

10.1166/jnn.2009.1246

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

A sonochemical method was used to synthesize carbon nanotube (CNT) in the presence of dichlorobenzene and ZnCl2 under ambient conditions. Structural characterizations were carried out using Raman spectroscopy, X-ray diffraction (XRD) and X-Ray photoelectron spectroscopy (XPS) which confirmed successful formation of CNT Thermogravimetric analysis shows reduction in amorphous carbon with increase in the sonication period. Morphological studies using field emission scanning electron microscope (FE-SEM) and High resolution transmission electron microscopy (HR-TEM) reveals the formation of combination of single and multiwall carbon nanotubes. The electronic band structural characterization using Ultra violet-visible-near infrared spectroscopy (UV-Vis/NIR) confirms the existence of metallic and semiconducting carbon nanotubes.

引用

页码：5940 / 5945

页数：6

共 36 条

[31] ON THE ORIGIN OF SONOLUMINESCENCE AND SONOCHEMISTRY [J].

SUSLICK, KS ;

DOKTYCZ, SJ ;

FLINT, EB .

ULTRASONICS, 1990, 28 (05) :280-290

[32] APPLICATIONS OF ULTRASOUND TO MATERIALS CHEMISTRY [J].

SUSLICK, KS .

MRS BULLETIN, 1995, 20 (04) :29-34

[33] ORGANOMETALLIC SONOCHEMISTRY [J].

SUSLICK, KS .

ADVANCES IN ORGANOMETALLIC CHEMISTRY, 1986, 25 :73-119

[34] Crystalline ropes of metallic carbon nanotubes [J].

Thess, A ;

Lee, R ;

Nikolaev, P ;

Dai, HJ ;

Petit, P ;

Robert, J ;

Xu, CH ;

Lee, YH ;

Kim, SG ;

Rinzler, AG ;

Colbert, DT ;

Scuseria, GE ;

Tomanek, D ;

Fischer, JE ;

Smalley, RE .

SCIENCE, 1996, 273 (5274) :483-487

[35] Resonant Raman spectroscopy of nanotubes [J].

Thomsen, C ;

Reich, S ;

Maultzsch, J .

PHILOSOPHICAL TRANSACTIONS OF THE ROYAL SOCIETY A-MATHEMATICAL PHYSICAL AND ENGINEERING SCIENCES, 2004, 362 (1824) :2337-2359

[36] Low-temperature growth of carbon nanotubes from the catalytic decomposition of carbon tetrachloride [J].

Vohs, JK ;

Brege, JJ ;

Raymond, JE ;

Brown, AE ;

Williams, GL ;

Fahlman, BD .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 2004, 126 (32) :9936-9937

← 1 2 3 4 →