Amperometric Detection of Glucose by Polyaniline-Activated Carbon Composite Carbon Paste Electrode

被引:0
作者
Colak, Ozlem [1 ]
Arslan, Halit [1 ]
Zengin, Huseyin [2 ]
Zengin, Gulay [2 ]
机构
[1] Gazi Univ, Fac Sci, Dept Chem, TR-06500 Ankara, Turkey
[2] Gaziantep Univ, Fac Arts & Sci, Dept Chem, Gaziantep, Turkey
来源
INTERNATIONAL JOURNAL OF ELECTROCHEMICAL SCIENCE | 2012年 / 7卷 / 08期
关键词
Glucose; glucose oxidase; biosensor; polyaniline (Pani); polyaniline activated carbon composite; carbon paste; BIOSENSOR; OXIDASE; FILM; NANOPARTICLES; MEMBRANE;
D O I
暂无
中图分类号
O646 [电化学、电解、磁化学];
学科分类号
081704 ;
摘要
In this study, a novel carbon paste electrode using the salt form of polyaniline (pani)-activated carbon composite sensitive to glucose, was prepared. Glucose oxidase enzyme was immobilized to modified carbon paste electrode by cross-linking with glutaraldehyde. Determination of glucose was carried out by the oxidation of enzymatically produced H2O2 at 0.4 V vs. Ag/AgCl. The effects of pH and temperature were investigated and optimum parameters were found to be 5.0 and 65 degrees C, respectively. The linear working range of the electrode was 5.0x10(-7) - 1.0x10(-5) M, R-2 = 0.980. The storage stability and operation stability of the enzyme electrode were also studied.
引用
收藏
页码:6988 / 6997
页数:10
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