4-[(E)-(5-Chloro-2-hydroxybenzylidene)amino]benzenesulfonamide

被引：6

作者：

Crohan, Zahid H. ^{[2
]}

Shad, Hazoor A. ^{[2
]}

Tahir, M. Nawaz ^{[1
]}

机构：

[1] Univ Sargodha, Dept Phys, Sargodha, Pakistan

[2] Bahauddin Zakariya Univ, Dept Chem, Multan 60800, Pakistan

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2009年 / 65卷

关键词：

X-RAY; SULFONAMIDES; BENZENESULFONAMIDE;

D O I：

10.1107/S1600536808040853

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

In the molecule of title compound, C13H11ClN2O3S, the aromatic rings are oriented at a dihedral angle of 12.27 (3)degrees. An intramolecular O-H center dot center dot center dot N hydrogen bond results in the formation of a planar (mean deviation 0.0083 angstrom) six-membered ring, which is nearly coplanar with the adjacent ring at a dihedral angle of 2.36 (13)degrees. In the sulfonamide group, the S atom is 0.457 (3) angstrom from the plane through the O and N atoms. In the crystal structure, intermolecular N-H center dot center dot center dot O hydrogen bonds link the molecules.

引用

页码：O57 / U1752

页数：9

共 16 条

[1] TABLES OF BOND LENGTHS DETERMINED BY X-RAY AND NEUTRON-DIFFRACTION .1. BOND LENGTHS IN ORGANIC-COMPOUNDS [J].

ALLEN, FH ;

KENNARD, O ;

WATSON, DG ;

BRAMMER, L ;

ORPEN, AG ;

TAYLOR, R .

JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 2, 1987, (12) :S1-S19

[2]

Bruker, 2007, APEX2 SAINT

[3]

Bruker, 2005, SADABS

[4]

Chohan ZH, 2008, J ENZYM INHIB MED CH, V23, P369, DOI [10.1080/14756360701585692, 10.1080/14756360701585692 ]

[5]

Chohan ZH, 2008, J ENZYM INHIB MED CH, V23, P240, DOI [10.1080/14756360701474913, 10.1080/14756360701474913 ]

[6] 4-{2-[(5-Chloro-2-hydroxybenzylidene)amino]ethyl}benzenesulfonamide [J].

Chohan, Zahid H. ;

Shad, Hazoor A. ;

Tahir, M. Nawaz ;

Khan, Islam Ullah .

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 :O725-U1512

[7] 4-(5-Chloro-2-hydroxybenzylideneamino)-N-(4,6-dimethylpyrimidin-2-yl) benzenesulfonamide [J].

Chohan, Zahid H. ;

Tahir, M. Nawaz ;

Shad, Hazoor A. ;

Khan, Islam Ullah .

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 :O648-U791

[8]

Chohan ZH, 2008, J ENZYM INHIB MED CH, V23, P120, DOI [10.1080/14756360701384195, 10.1080/14756360701384195 ]

[9]

Farrugia L. J., 1999, J. Appl. Crystallogr, V32, P837, DOI [DOI 10.1107/S0021889812029111, DOI 10.1107/S0021889899006020]

[10]

Farrujia LJ., 1997, J APPL CRYSTALLOGR, V30, P565, DOI [10.1107/S0021889897003117, DOI 10.1107/S0021889897003117]

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