The dedicated high-resolution grazing-incidence X-ray scattering beamline 8-ID-E at the Advanced Photon Source

被引:113
作者
Jiang, Zhang [1 ]
Li, Xuefa [1 ]
Strzalka, Joseph [1 ]
Sprung, Michael [1 ]
Sun, Tao [1 ]
Sandy, Alec R. [1 ]
Narayanan, Suresh [1 ]
Lee, Dong Ryeol [1 ]
Wang, Jin [1 ]
机构
[1] Argonne Natl Lab, Xray Sci Div, Argonne, IL 60439 USA
关键词
X-ray scattering; grazing incidence; coherence; beamline; high resolution; BLOCK-COPOLYMERS; SURFACE-LAYERS; THIN-FILMS; ANGLE; WAVE; MONOLAYERS; MEMBRANES; DESIGN;
D O I
10.1107/S0909049512022017
中图分类号
TH7 [仪器、仪表];
学科分类号
0804 ; 080401 ; 081102 ;
摘要
As an increasingly important structural-characterization technique, grazing-incidence X-ray scattering (GIXS) has found wide applications for in situ and real-time studies of nanostructures and nanocomposites at surfaces and interfaces. A dedicated beamline has been designed, constructed and optimized at beamline 8-ID-E at the Advanced Photon Source for high-resolution and coherent GIXS experiments. The effectiveness and applicability of the beamline and the scattering techniques have been demonstrated by a host of experiments including reflectivity, grazing-incidence static and kinetic scattering, and coherent surface X-ray photon correlation spectroscopy. The applicable systems that can be studied at 8-ID-E include liquid surfaces and nanostructured thin films.
引用
收藏
页码:627 / 636
页数:10
相关论文
共 38 条
  • [1] Convective Assembly of 2D Lattices of Virus-like Particles Visualized by In-Situ Grazing-Incidence Small-Angle X-Ray Scattering
    Ashley, Carlee E.
    Dunphy, Darren R.
    Jiang, Zhang
    Carnes, Eric C.
    Yuan, Zhen
    Petsev, Dimiter N.
    Atanassov, Plamen B.
    Velev, Orlin D.
    Sprung, Michael
    Wang, Jin
    Peabody, David S.
    Brinker, C. Jeffrey
    [J]. SMALL, 2011, 7 (08) : 1043 - 1050
  • [2] DUTTA P, 1981, PHYS REV LETT, V47, P50, DOI 10.1103/PhysRevLett.47.50
  • [3] X-RAY FLUX ENHANCEMENT IN THIN-FILM WAVE-GUIDES USING RESONANT BEAM COUPLERS
    FENG, YP
    SINHA, SK
    DECKMAN, HW
    HASTINGS, JB
    SIDDONS, DP
    [J]. PHYSICAL REVIEW LETTERS, 1993, 71 (04) : 537 - 540
  • [4] Structure and dynamics correlations of photoinduced charge separation in rigid conjugated linear donor-acceptor dyads towards photovoltaic applications
    Guo, Jianchang
    Liang, Yongye
    Xiao, Shengqian
    Szarko, Jodi M.
    Sprung, Michael
    Mukhopadhyay, Mrinmay K.
    Wang, Jin
    Yu, Luping
    Chen, Lin X.
    [J]. NEW JOURNAL OF CHEMISTRY, 2009, 33 (07) : 1497 - 1507
  • [5] Observation of a low-viscosity interface between immiscible polymer layers
    Hu, Xuesong
    Jiang, Zhang
    Narayanan, Suresh
    Jiao, Xuesong
    Sandy, Alec R.
    Sinha, Sunil K.
    Lurio, Laurence B.
    Lal, Jyotsana
    [J]. PHYSICAL REVIEW E, 2006, 74 (01):
  • [6] Self-Assembled Nano layers of Conjugated Si lane with π-π Interlocking
    Jiang, Jinyue
    Lima, Ocelio V.
    Pei, Yong
    Jiang, Zhang
    Chen, Ziguang
    Yu, Chichao
    Wang, Jin
    Zeng, Xiao Cheng
    Forsythe, Eric
    Tan, Li
    [J]. ACS NANO, 2010, 4 (07) : 3773 - 3780
  • [7] Waveguide-enhanced grazing-incidence small-angle x-ray scattering of buried nanostructures in thin films
    Jiang, Zhang
    Lee, Dong Ryeol
    Narayanan, Suresh
    Wang, Jin
    Sinha, Sunil K.
    [J]. PHYSICAL REVIEW B, 2011, 84 (07)
  • [8] Capturing the Crystalline Phase of Two-Dimensional Nanocrystal Superlattices in Action
    Jiang, Zhang
    Lin, Xiao-Min
    Sprung, Michael
    Narayanan, Suresh
    Wang, Jin
    [J]. NANO LETTERS, 2010, 10 (03) : 799 - 803
  • [9] IsGISAXS:: a program for grazing-incidence small-angle X-ray scattering analysis of supported islands
    Lazzari, R
    [J]. JOURNAL OF APPLIED CRYSTALLOGRAPHY, 2002, 35 : 406 - 421
  • [10] In-situ grazing incidence small-angle X-ray scattering studies on nanopore evolution in low-k organosilicate dielectric thin films
    Lee, B
    Yoon, J
    Oh, W
    Hwang, Y
    Heo, K
    Jin, KS
    Kim, J
    Kim, KW
    Ree, M
    [J]. MACROMOLECULES, 2005, 38 (08) : 3395 - 3405