In-situ X-ray diffraction measurement of electrodeposition process in molten salts

被引：0

作者：

Kajinami, A

Deki, S

Umesaki, N

Sato, M

Myochin, M

机构：

[1] Kobe Univ, Fac Engn, Kobe, Hyogo, Japan

[2] Japan Synchrotron Radiat Res Inst, Sayo, Hyogo, Japan

[3] Japan Nucl Cycle Dev Inst, Ibaraki, Japan

来源：

NEW FRONTIERS OF PROCESSING AND ENGINEERING IN ADVANCED MATERIALS | 2005年 / 502卷

关键词：

in-situ X-ray diffraction; electrodeposition process; molten salt; carbon electrode; synchrotron radiation; nickel metal;

D O I：

10.4028/www.scientific.net/MSF.502.335

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

In-situ X-ray diffraction (XRD) method has been developed for the observation of elctrodeposition process in molten NaCl-2CsCl salt to investigate the mechanism of pyrochemical process of nuclear fuel reprocessing system. In this paper, the scattered X-ray beam from electrodepositing nickel in NaCl-2CsCl melt was measured by the reflection mode at BL19B2 beamline of SPring-8 as the preliminary experiment. The time dependence of the electrodepositing nickel in NaCl-2CsCl melt at 923K was investigated by the in-situ XRD measurements.

引用

页码：335 / 338

页数：4