Hydrothermal preparation and characterization of octadecahedron Fe3O4 film

被引:9
作者
Chen, Jie [1 ]
Huang, Kelong [1 ]
Liu, Suqin [1 ]
机构
[1] Cent S Univ, Coll Chem & Chem Engn, Changsha 410083, Hunan, Peoples R China
关键词
Hydrothermal method; Fe3O4; film; Octadecahedron; IRON-OXIDE; THIN-FILMS; SHAPE; MAGNETITE; CHEMISTRY; GROWTH;
D O I
10.1016/j.jallcom.2009.03.092
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
A 'green' hydrothermal process was used to prepare Fe3O4 film on steel foil using FeSO4 center dot 7H(2)O as the iron source and H2O2 as the oxidant. X-ray diffraction (XRD), scanning electron microscopy (SEM) and transmission electron microscope (TEM) were employed to characterize the film. The results showed that the film was composed of fine particles with regularly octadecahedron morphology. The average diameter of the particles ranged from 300 nm to 1 mu m. Furthermore, the probable mechanism for the formation of Fe3O4 film with octadecahedron morphology was suggested. (C) 2009 Published by Elsevier B.V.
引用
收藏
页码:207 / 210
页数:4
相关论文
共 13 条
  • [1] Novel photocatalyst: Titania-coated magnetite. Activity and photodissolution
    Beydoun, D
    Amal, R
    Low, GKC
    McEvoy, S
    [J]. JOURNAL OF PHYSICAL CHEMISTRY B, 2000, 104 (18) : 4387 - 4396
  • [2] EERENSTEIN W, 2003, J MAGN MAGN MATER, V73, P258
  • [3] Size-controlled growth of Co3O4 nanocubes
    Feng, J
    Zeng, HC
    [J]. CHEMISTRY OF MATERIALS, 2003, 15 (14) : 2829 - 2835
  • [4] KRAUSE MK, 2002, J MAGN MAGN MATER, V1097, P242
  • [5] One-dimensional nanostructures:: Chemistry, physics & applications
    Lieber, CM
    [J]. SOLID STATE COMMUNICATIONS, 1998, 107 (11) : 607 - 616
  • [6] DIRECT PREPARATION OF GAMMA-FE2O3 THIN-FILM RECORDING MEDIA BY REACTIVE RF-SPUTTERING TECHNIQUE
    OHTA, S
    TERADA, A
    [J]. THIN SOLID FILMS, 1986, 143 (01) : 73 - 82
  • [7] Nanobelts of semiconducting oxides
    Pan, ZW
    Dai, ZR
    Wang, ZL
    [J]. SCIENCE, 2001, 291 (5510) : 1947 - 1949
  • [8] Colloidal nanocrystal shape and size control: The case of cobalt
    Puntes, VF
    Krishnan, KM
    Alivisatos, AP
    [J]. SCIENCE, 2001, 291 (5511) : 2115 - 2117
  • [9] Thin films of iron oxide by low pressure MOCVD using a novel precursor:: tris(t-butyl-3-oxo-butanoato)iron(III)
    Shalini, K
    Subbanna, GN
    Chandrasekaran, S
    Shivashankar, SA
    [J]. THIN SOLID FILMS, 2003, 424 (01) : 56 - 60
  • [10] Shape-controlled synthesis of gold and silver nanoparticles
    Sun, YG
    Xia, YN
    [J]. SCIENCE, 2002, 298 (5601) : 2176 - 2179