Hydrodistillation-headspace solvent microextraction:: An efficient method for analysis of the essential oil from the seeds of Foeniculum vulgare Mill.

被引：12

作者：

Salehi, P. ^{[1
]}

Asghari, B. ^{[1
]}

Mohammadi, F. ^{[1
]}

机构：

[1] Shahid Beheshti Univ, Med Plants & Drugs Res Inst, Dept Phytochem, Tehran, Iran

来源：

CHROMATOGRAPHIA | 2007年 / 65卷 / 1-2期

关键词：

gas chromatography; headspace solvent microextraction; hydrodistillation; Foeniculum vulgare Mill; essential oil;

D O I：

10.1365/s10337-006-0102-9

中图分类号：

Q5 [生物化学];

学科分类号：

071010 ; 081704 ;

摘要：

Hydrodistillation-headspace solvent microextraction (HD-HSME) has been used for isolation and preconcentration of the essential oil from the seeds of Foeniculum vulgare Mill. The effect on extraction efficiency of different conditions, for example sample mass, extraction time, micro-drop volume, and choice of solvent, was studied and all were optimized. The results were compared with those from hydrodistillation, as reference method. Fourteen compounds were identified; the main components were trans-anethole (70.4%), fenchone (9.3%), and p-allylanisole (8.8%). The results were in good agreement with those obtained by hydrodistillation.

引用

页码：119 / 122

页数：4

共 27 条

[1]

Adams R., 2001, Identification of essential oil components by gas chromatography/quadrupole mass spectrometry

[2]

Amjad Hassan, 2000, American Journal of Gastroenterology, V95, P2491

[3] SOLID-PHASE MICROEXTRACTION WITH THERMAL-DESORPTION USING FUSED-SILICA OPTICAL FIBERS [J].