The sinterability of yttria-tetragonal zirconia polycrystals (Y-TZP) containing small amounts of MnO2 as sintering aid was investigated over the temperature range of 1250-1500 degrees C. Sintered samples were evaluated to determine bulk density, Young's modulus, Vickers hardness and fracture toughness. In addition, the tetragonal phase stability of selected samples was evaluated by subjecting the samples to hydrothermal ageing in superheated steam at 180 degrees C/10 bar for up to 24 h. The results showed that the addition of MnO2, particularly >= 0.3 wt% was effective in aiding densification, improving the matrix stiffness and hardness when compared to the undoped Y-TZP sintered at temperatures below 1350 degrees C. On the other hand, the fracture toughness of Y-TZP was unaffected by MnO2 addition except for the 1 wt% MnO2-doped Y-TZP samples sintered above 1400 degrees C. The hydrothermal ageing resistance of Y-TZP was significantly improved with the additions of MnO2 in the Y-TZP matrix. (C) 2007 Elsevier Ltd and Techna Group S.r.l. All rights reserved.
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American Society for Testing and Materials ASTM G32, 1998, ANN BOOK ASTM STAND
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Inst Natl Sci Appl, Associate Res Unit 5510, Dept Res Met & Phys Properties Mat, F-69621 Villeurbanne, FranceInst Natl Sci Appl, Associate Res Unit 5510, Dept Res Met & Phys Properties Mat, F-69621 Villeurbanne, France
Chevalier, J
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Deville, S
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Deville, S
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Münch, E
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Münch, E
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Jullian, R
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Inst Natl Sci Appl, Associate Res Unit 5510, Dept Res Met & Phys Properties Mat, F-69621 Villeurbanne, FranceInst Natl Sci Appl, Associate Res Unit 5510, Dept Res Met & Phys Properties Mat, F-69621 Villeurbanne, France
Jullian, R
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Lair, F
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Natl Inst Appl Sci GEMPPM INSA, Dept Mat Sci, Associate Res Unit 5510, F-69621 Villeurbanne, FranceNatl Inst Appl Sci GEMPPM INSA, Dept Mat Sci, Associate Res Unit 5510, F-69621 Villeurbanne, France
Deville, S
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Chevalier, J
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Chevalier, J
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Gremillard, L
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Inst Natl Sci Appl, Associate Res Unit 5510, Dept Res Met & Phys Properties Mat, F-69621 Villeurbanne, FranceInst Natl Sci Appl, Associate Res Unit 5510, Dept Res Met & Phys Properties Mat, F-69621 Villeurbanne, France
Chevalier, J
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Deville, S
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Inst Natl Sci Appl, Associate Res Unit 5510, Dept Res Met & Phys Properties Mat, F-69621 Villeurbanne, FranceInst Natl Sci Appl, Associate Res Unit 5510, Dept Res Met & Phys Properties Mat, F-69621 Villeurbanne, France
Deville, S
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Münch, E
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Inst Natl Sci Appl, Associate Res Unit 5510, Dept Res Met & Phys Properties Mat, F-69621 Villeurbanne, FranceInst Natl Sci Appl, Associate Res Unit 5510, Dept Res Met & Phys Properties Mat, F-69621 Villeurbanne, France
Münch, E
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Jullian, R
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Inst Natl Sci Appl, Associate Res Unit 5510, Dept Res Met & Phys Properties Mat, F-69621 Villeurbanne, FranceInst Natl Sci Appl, Associate Res Unit 5510, Dept Res Met & Phys Properties Mat, F-69621 Villeurbanne, France
Jullian, R
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Lair, F
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Inst Natl Sci Appl, Associate Res Unit 5510, Dept Res Met & Phys Properties Mat, F-69621 Villeurbanne, FranceInst Natl Sci Appl, Associate Res Unit 5510, Dept Res Met & Phys Properties Mat, F-69621 Villeurbanne, France
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Natl Inst Appl Sci GEMPPM INSA, Dept Mat Sci, Associate Res Unit 5510, F-69621 Villeurbanne, FranceNatl Inst Appl Sci GEMPPM INSA, Dept Mat Sci, Associate Res Unit 5510, F-69621 Villeurbanne, France
Deville, S
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Chevalier, J
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Natl Inst Appl Sci GEMPPM INSA, Dept Mat Sci, Associate Res Unit 5510, F-69621 Villeurbanne, FranceNatl Inst Appl Sci GEMPPM INSA, Dept Mat Sci, Associate Res Unit 5510, F-69621 Villeurbanne, France
Chevalier, J
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Gremillard, L
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Natl Inst Appl Sci GEMPPM INSA, Dept Mat Sci, Associate Res Unit 5510, F-69621 Villeurbanne, FranceNatl Inst Appl Sci GEMPPM INSA, Dept Mat Sci, Associate Res Unit 5510, F-69621 Villeurbanne, France