Magnesium Borate Synthesis by Microwave Energy: A New Method

被引:18
作者
Kipcak, Azmi Seyhun [1 ]
Derun, Emek Moroydor [1 ]
Piskin, Sabriye [1 ]
机构
[1] Yildiz Tech Univ, Fac Chem & Met Engn, Dept Chem Engn, TR-34210 Istanbul, Turkey
关键词
MG2B2O5; NANOWIRES;
D O I
10.1155/2013/329238
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Magnesium borates are one of the major groups of boron minerals that have important properties such as high heat and corrosion resistances and high coefficients of elasticity. In this study, magnesium borate minerals are synthesized using boric acid and magnesium oxide with a new method of microwave, and the synthesized minerals are characterized by various analysis techniques. The results show that pure, "magnesium borate hydrate" minerals are obtained at the end of various steps. The characterization of the products is determined with the techniques of X-Ray Diffraction (XRD), Fourier Transform Infrared Spectroscopy (FTIR), Raman Spectroscopy, and Scanning Electron Microscopy (SEM). Additionally, overall "magnesium borate hydrate" yields are calculated and found about 67% at 270W, 8 minutes and 360W, 3 minutes of reaction times, respectively.
引用
收藏
页数:6
相关论文
共 18 条
[1]  
[Anonymous], 2012, BOR SECT REP
[2]  
Ay E., 2006, THESIS BALIKESIR U B
[3]   The synthesis and microwave dielectric properties of Mg3B2O6 and Mg2B2O5 ceramics [J].
Dosler, Urban ;
Krzmanc, Marjeta Macek ;
Suvorov, Danilo .
JOURNAL OF THE EUROPEAN CERAMIC SOCIETY, 2010, 30 (02) :413-418
[4]   Synthesis of magnesium borate nanorods [J].
Elssfah, E. M. ;
Elsanousi, A. ;
Zhang, J. ;
Song, H. S. ;
Tang, Chengcun .
MATERIALS LETTERS, 2007, 61 (22) :4358-4361
[5]  
Erdogan H., 2008, THESIS HACETTEPE U A
[6]  
Fogler H. S., 1999, ELEMENT CHEM REACTIO
[7]  
Guler H., 2009, P 4 INT BOR S ESK TU
[8]  
Kipcak A. S., 2012, INT C CHEM ENG ICCE
[9]   A new route for the synthesis of Mg2B2O5 nanorods by mechano-chemical and sintering process [J].
Li, Shuang ;
Fang, Xuan ;
Leng, Jing ;
Shen, Hongzhi ;
Fan, Ya ;
Xu, Dapeng .
MATERIALS LETTERS, 2010, 64 (02) :151-153
[10]   Synthesis of magnesium borate (Mg2B2O5) nanowires by chemical vapor deposition method [J].
Li, Y ;
Fan, ZY ;
Lu, JG ;
Chang, RPH .
CHEMISTRY OF MATERIALS, 2004, 16 (13) :2512-2514