Low-temperature crystal structure of the inclusion compound {[N(CH3)(4)](+)(Cl)(2)(-)}center dot CH3CN center dot H2O

被引：0
作者：
Minkwitz, R
Brochler, R
Preut, H
机构：
来源：
ZEITSCHRIFT FUR NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES | 1996年 / 51卷 / 04期
关键词：
preparation; crystal structure; inclusion compound;
D O I：
暂无
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
The crystal structure of {[N(CH3)(4)Cl-+(-)](2)}. CH3CN . H2O is reported. Crystalls are orthorhombic, space group Pnma, with a = 1622.9(15), b = 671.3(6), c = 1511.2(11) pm, V = 1646(2) 10(6) pm(3) and Z = 4.
引用
收藏
页码：599 / 601
页数：3
相关论文
共 19 条
[11]  
MINKWITZ R, UNPUB
[12]   FLUORIDES AND FLUORO ACIDS .11. POLY(HYDROGEN FLUORIDES) WITH THE TETRAMETHYLAMMONIUM CATION - PREPARATION, STABILITY RANGES, CRYSTAL-STRUCTURES, [HNFN+1]- ANION HOMOLOGY, HYDROGEN-BONDING F-H=F [J].
MOOTZ, D ;
BOENIGK, D .
ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE, 1987, 544 (01) :159-166
[13]   PARST - A SYSTEM OF FORTRAN ROUTINES FOR CALCULATING MOLECULAR-STRUCTURE PARAMETERS FROM RESULTS OF CRYSTAL-STRUCTURE ANALYSES [J].
NARDELLI, M .
COMPUTERS & CHEMISTRY, 1983, 7 (03) :95-98
[14]   DISORDER AND POLYMORPHISM OF TETRAMETHYLAMMONIUM CHLORIDE [J].
PISTORIUS, CW ;
GIBSON, AAV .
JOURNAL OF SOLID STATE CHEMISTRY, 1973, 8 (02) :126-131
[15]  
SHELDRICK GM, 1987, SHELXTL PLUS RELEASE
[16]  
SHELDRICK GM, 1993, SHELX93 PROGRAM REFI
[17]  
SPEK AL, 1982, COMPUTATIONAL CRYSTA, P528
[18]  
WYCKOFF RWG, 1962, CRYSTAL STRUCTURES, V1
[19]  
YANG Y, 1980, ACTA CRYSTALLOGR B, V36, P1523
12