Correlation NMR spectroscopy involving quadrupolar nuclei

被引:40
作者
Amoureux, J. P. [1 ]
Trebosc, J. [1 ]
Delevoye, L. [1 ]
Lafon, O. [1 ]
Hu, B. [1 ]
Wang, Q. [1 ,2 ,3 ]
机构
[1] Univ Lille, CNRS 8181, UCCS, FR-59652 Villeneuve Dascq, France
[2] Chinese Acad Sci, Wuhan Inst Phys & Math, Wuhan Ctr Magnet Resonance, State Key Lab Magnet Resonance & Atom & Mol Phys, Wuhan 430071, Peoples R China
[3] Chinese Acad Sci, Grad Sch, Beijing, Peoples R China
关键词
Solid-state NMR; Quadrupolar nuclei; Through-space connectivities; Through-bond connectivities; QUANTUM CROSS-POLARIZATION; SOLID-STATE NMR; ECHO DOUBLE-RESONANCE; ANGLE-SPINNING NMR; RESOLUTION HETERONUCLEAR CORRELATION; DIPOLAR INTERACTIONS; SPIN-1/2; NUCLEI; ROTARY RESONANCE; N-14; NMR; COHERENCE TRANSFER;
D O I
10.1016/j.ssnmr.2008.11.004
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
We review the recent developments proposed for integer or half-integer quadrupolar nuclei, focussing on the methods to observe them under high-resolution and to analyze their through-space and through-bond connectivities. (C) 2008 Elsevier Inc. All rights reserved.
引用
收藏
页码:12 / 18
页数:7
相关论文
共 66 条
[1]  
Abragam A., 1961, The principles of nuclear magnetism
[2]   Measurement of through-space connectivities between spin-1/2 and quadrupolar nuclei in solid-state NMR: the TEDOR-MQMAS method [J].
Amoureux, J. P. ;
Trebosc, J. ;
Tricot, G. .
MAGNETIC RESONANCE IN CHEMISTRY, 2007, 45 :S187-S191
[3]   High-resolution 14N-edited 1H-13C correlation NMR experiment to study biological solids [J].
Amoureux, Jean-Paul ;
Trebosc, Julien ;
Hu, Bingwen ;
Halpern-Manners, Nicholas ;
Antonijevic, Sasa .
JOURNAL OF MAGNETIC RESONANCE, 2008, 194 (02) :317-320
[4]   Enhanced resolution in proton solid-state NMR with very-fast MAS experiments [J].
Amoureux, Jean-Paul ;
Hu, Bingwen ;
Trebosc, Julien .
JOURNAL OF MAGNETIC RESONANCE, 2008, 193 (02) :305-307
[5]   Rapid analysis of isotopically unmodified amino acids by high-resolution 14N-edited 1H-13C correlation NMR spectroscopy [J].
Amoureux, Jean-Paul ;
Wang, Qiang ;
Hu, Bingwen ;
Lafon, Olivier ;
Trebosc, Julien ;
Deng, Feng .
CHEMICAL COMMUNICATIONS, 2008, (48) :6525-6527
[6]   Z filtering in MQMAS NMR [J].
Amoureux, JP ;
Fernandez, C ;
Steuernagel, S .
JOURNAL OF MAGNETIC RESONANCE SERIES A, 1996, 123 (01) :116-118
[7]   Implementing SPAM into STMAS: A net sensitivity improvement in high-resolution NMR of quadrupolar nuclei [J].
Amoureux, JP ;
Delevoye, L ;
Fink, G ;
Taulelle, F ;
Flambard, A ;
Montagne, L .
JOURNAL OF MAGNETIC RESONANCE, 2005, 175 (02) :285-299
[8]   Increasing the sensitivity of 2D high-resolution NMR methods applied to quadrupolar nuclei [J].
Amoureux, JP ;
Delevoye, L ;
Steuernagel, S ;
Gan, Z ;
Ganapathy, S ;
Montagne, L .
JOURNAL OF MAGNETIC RESONANCE, 2005, 172 (02) :268-278
[9]   Theoretical and experimental assessment of single- and multiple-quantum cross-polarization in solid state NMR [J].
Amoureux, JP ;
Pruski, M .
MOLECULAR PHYSICS, 2002, 100 (10) :1595-1613
[10]   Probing amide bond nitrogens in solids using 14N NMR spectroscopy [J].
Department of Chemistry, University of California, Berkeley, 1 Cyclotron Road, Building 11-D64, Berkeley, CA 94720, United States ;
不详 .
Solid State Nucl Magn Reson, 2008, 4 (82-87) :82-87