Crystal structure of N-[1-(2,6-dichloro-4-trifluoromethyl)phenyl-3-cyano-1H-pyrazol-5-yl]-N′-4-phenylacetyl thiourea, C20H12Cl2F3N5OS

被引:0
作者
Xu, Li [1 ]
Zhu, Pengfei [1 ]
Xie, Huamei [1 ]
Zhang, Xiao-Hong [1 ]
Zhong, Ping [1 ,2 ]
机构
[1] Wenzhou Univ, Coll Chem & Mat Sci, Wenzhou 325027, Zhejiang, Peoples R China
[2] Wenzhou Univ, Oujiang Coll, Wenzhou 325027, Zhejiang, Peoples R China
来源
ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES | 2012年 / 227卷 / 03期
基金
中国国家自然科学基金;
关键词
FIPRONIL;
D O I
10.1524/ncrs.2012.0183
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
C20H12Cl2F3N5Os, triclinic, P (1) over bar (no. 2), a = 12.300(3) angstrom, b = 14.379(3) angstrom, c = 14.496(3) angstrom, alpha = 69.511(4)degrees, beta = 72.163(4)degrees, gamma = 70.491(4)degrees, V = 2211.0 angstrom(3), Z = 4, R-gt(F) = 0.0611, wR(ref)(F-2) = 0.1679, T = 298 K.
引用
收藏
页码:401 / 403
页数:3
相关论文
共 9 条
  • [1] Degradation of fipronil in anaerobic sediments and the effect on porewater concentrations
    Brennan, Amanda A.
    Harwood, Amanda D.
    You, Jing
    Landrum, Peter F.
    Lydy, Michael J.
    [J]. CHEMOSPHERE, 2009, 77 (01) : 22 - 28
  • [2] Toxicity and neurophysiological effects of fipronil and its oxidative sulfone metabolite on European corn borer larvae (Lepidoptera: Crambidae)
    Durham, EW
    Scharf, ME
    Siegfried, BD
    [J]. PESTICIDE BIOCHEMISTRY AND PHYSIOLOGY, 2001, 71 (02) : 97 - 106
  • [3] Gong YX, 2006, CHINESE J ORG CHEM, V26, P360
  • [4] HATTON LR, 1993, Patent No. 5232940
  • [5] New chemistry with old ligands:: N-alkyl- and N,N-dialkyl-N′-acyl(aroyl)thioureas in co-ordination, analytical and process chemistry of the platinum group metals
    Koch, KR
    [J]. COORDINATION CHEMISTRY REVIEWS, 2001, 216 : 473 - 488
  • [6] MADAN VK, 1991, J INDIAN CHEM SOC, V68, P162
  • [7] A short history of SHELX
    Sheldrick, George M.
    [J]. ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2008, 64 : 112 - 122
  • [8] Xue SJ, 2004, CHINESE J ORG CHEM, V24, P686
  • [9] Structural and spectral studies of N-(4-chloro)benzoyl-N′-2-tolylthiourea
    Zhou, WQ
    Leng, KS
    Yong, Z
    Lu, L
    [J]. JOURNAL OF MOLECULAR STRUCTURE, 2003, 657 (1-3) : 215 - 223