A single-source route to CdS nanorods

被引：78
作者：
Nair, PS
Radhakrishnan, T
Revaprasadu, N
Kolawole, GA
O'Brien, P
机构：
[1] Univ Zululand, Dept Chem, ZA-3886 Kwa Dlangezwa, South Africa
[2] Univ Manchester, Dept Chem, Manchester M13 9PL, Lancs, England
[3] Univ Manchester, Manchester Mat Sci Ctr, Manchester M13 9PL, Lancs, England
来源：
CHEMICAL COMMUNICATIONS | 2002年 / 06期
关键词：
D O I：
10.1039/b200434h
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
We report the preparation of CdS nanorods using a thiosemicarbazide complex of cadmium [Cd(NH2CSNHNH2)(2)Cl-2]. The precursor was decomposed in tri-n-octylphosphine oxide (TOPO) at 280 degreesC to give TOPO capped CdS nanoparticles; nano-dimensional rods of the material are clearly visible in transmission electron microscopy (TEM); the particles have been further characterised by X-ray diffraction (XRD) and selected area electron diffraction (SAED) and optical measurements.
引用
收藏
页码：564 / 565
页数：2
相关论文
共 19 条
[1]   Simple solution-phase synthesis of soluble CdS and CdSe nanorods [J].
Chen, CC ;
Chao, CY ;
Lang, ZH .
CHEMISTRY OF MATERIALS, 2000, 12 (06) :1516-+
[2]  
Cullity BD, 1978, ELEMENTS XRAY DIFFRA
[3]   Structure and photophysics of semiconductor nanocrystals [J].
Eychmüller, A .
JOURNAL OF PHYSICAL CHEMISTRY B, 2000, 104 (28) :6514-6528
[4]   HIGH-RATE, GAS-PHASE GROWTH OF MOS2 NESTED INORGANIC FULLERENES AND NANOTUBES [J].
FELDMAN, Y ;
WASSERMAN, E ;
SROLOVITZ, DJ ;
TENNE, R .
SCIENCE, 1995, 267 (5195) :222-225
[5]   Metal nanowires and intercalated metal layers in single-walled carbon nanotube bundles [J].
Govindaraj, A ;
Satishkumar, BC ;
Nath, M ;
Rao, CNR .
CHEMISTRY OF MATERIALS, 2000, 12 (01) :202-205
[6]   Synthesis of gallium nitride nanorods through a carbon nanotube-confined reaction [J].
Han, WQ ;
Fan, SS ;
Li, QQ ;
Hu, YD .
SCIENCE, 1997, 277 (5330) :1287-1289
[7]   Synthesis of silicon nitride nanorods using carbon nanotube as a template [J].
Han, WQ ;
Fan, SS ;
Li, QQ ;
Gu, BL ;
Zhang, XB ;
Yu, DP .
APPLIED PHYSICS LETTERS, 1997, 71 (16) :2271-2273
[8]   Air-stable single-source precursors for the synthesis of chalcogenide semiconductor nanoparticles [J].
Malik, MA ;
Revaprasadu, N ;
O'Brien, P .
CHEMISTRY OF MATERIALS, 2001, 13 (03) :913-920
[9]   Synthesis of soluble and processable rod-, arrow-, teardrop-, and tetrapod-shaped CdSe nanocrystals [J].
Manna, L ;
Scher, EC ;
Alivisatos, AP .
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 2000, 122 (51) :12700-12706
[10]   Convenient microemulsion route to star-shaped cadmium sulfide pattern at room temperature [J].
Mo, X ;
Wang, CY ;
Hao, LY ;
You, M ;
Zhu, YR ;
Chen, ZY ;
Hu, Y .
MATERIALS RESEARCH BULLETIN, 2001, 36 (11) :1925-1930
12