Synthesis of symmetric anhydrides using visible light-mediated photoredox catalysis

被引：66
|
作者：
Konieczynska, Marlena D. [1 ]
Dai, Chunhui [1 ]
Stephenson, Corey R. J. [1 ]
机构：
[1] Boston Univ, Dept Chem, Boston, MA 02215 USA
来源：
ORGANIC & BIOMOLECULAR CHEMISTRY | 2012年 / 10卷 / 23期
基金：
美国国家科学基金会;
关键词：
CARBOXYLIC-ACID ANHYDRIDES; OXIDATION; EFFICIENT; PHASE; MILD; PHOTOCATALYSIS; CHLORIDES; REAGENTS; COMPLEX; HALIDES;
D O I：
10.1039/c2ob25463h
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
A new approach to anhydride formation is reported via activation of C-O bonds by the Vilsmeier-Haack reagent formed by Ru(bpy)(3)Cl-2 and CBr4 in DMF. Various aryl and alkyl carboxylic acids are converted to the corresponding anhydrides in excellent yields.
引用
收藏
页码：4509 / 4511
页数：3
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