Facile preparation of continuous indium metal-organic framework thin films on indium tin oxide glass

被引：13
|
作者：
Dou, Zhongshang [1 ]
Yu, Jiancan [1 ]
Xu, Hui [1 ]
Cui, Yuanjing [1 ]
Yang, Yu [1 ]
Qian, Guodong [1 ]
机构：
[1] Zhejiang Univ, Dept Mat Sci & Engn, Cyrus Tang Ctr Sensor Mat & Applicat, State Key Lab Silicon Mat, Hangzhou 310027, Zhejiang, Peoples R China
来源：
THIN SOLID FILMS | 2013年 / 544卷
基金：
中国国家自然科学基金;
关键词：
Metal-organic frameworks; Indium; Thin film; Solvothermal growth; MEMBRANE; SEPARATION; MOF;
D O I：
10.1016/j.tsf.2013.03.095
中图分类号：
T [工业技术];
学科分类号：
08 ;
摘要：
Continuous indium metal-organic framework thin films of In12O(OH)(12)[(OH)(4)center dot(H2O)(5))][BTC](6) (MIL-96(In)) (BTC = 1,3,5-benzenetricarboxylate) were prepared on indium tin oxide glass by in situ solvothermal growth method. The structure of the films was confirmed by X-ray diffraction. The growth process and the possible growth mechanism of MIL-96(In) films were investigated by a scanning electron microscopy. Furthermore, the influence of the reaction conditions on the morphology and thickness of films was studied. The best crack-free, continuous film with thickness of approximate 6 mu m was obtained at the proper concentrations of InCl3 and H3BTC of 25.0 mmol.l(1) at 100 degrees C for 12 h. (C) 2013 Elsevier B. V. All rights reserved.
引用
收藏
页码：296 / 300
页数：5
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