Cadmium-sensitive electrode based on tetracetone derivatives of p-tert-butylcalix[8]arene

被引：17

作者：

Dernane, C. ^{[1
]}

Zazoua, A. ^{[1
]}

Kazane, I. ^{[1
]}

Jaffrezic-Renault, N. ^{[2
]}

机构：

[1] Univ Jijel, Lab Mat Elaborat Proprietes Applicat, Ouled Aissa 18000, Jijel, Algeria

[2] Univ Lyon 1, LSA UMR CNRS 5180, F-69622 Villeurbanne, France

来源：

MATERIALS SCIENCE & ENGINEERING C-MATERIALS FOR BIOLOGICAL APPLICATIONS | 2013年 / 33卷 / 07期

关键词：

Calix[8]arene; Cadmium-sensitive electrode; Impedance spectroscopy; Sensors; ISFET SENSORS; ION DETECTION; THIN-FILMS; CALIXARENE; SPECTROMETRY; CHEMOSENSOR; FLUORESCENT; MERCURY(II); MEMBRANE; PROSTATE;

D O I：

10.1016/j.msec.2013.04.049

中图分类号：

TB3 [工程材料学]; R318.08 [生物材料学];

学科分类号：

0805 ; 080501 ; 080502 ;

摘要：

The performance of a cadmium-sensitive electrode based on the tetracetone derivatives of p-tert butylcalix [8]arene was investigated. The ion-sensitivity of the calix[8]arene was examined via cyclic voltammetry (CV), electrochemical impedance spectroscopy (EIS), X-ray photoelectron spectrometry, UV/Vis spectroscopy and FT-IR spectroscopy. The sensitive membrane containing the active ionophore was cast onto the surface of a gold electrode. The electrode exhibited a linear relationship between the charge transfer resistance (R-ct) and the logarithm of the detected ion concentration. The cathodic peak at a potential of 0.56 V increased linearly as the Cd2+ ion concentration increased. The detection limit of the device reached 10(-7) M with high sensitivity toward cadmium. (C) 2013 Elsevier B.V. All rights reserved.

引用

页码：3638 / 3643

页数：6

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