Cadmium-sensitive electrode based on tetracetone derivatives of p-tert-butylcalix[8]arene

被引：17
|
作者：
Dernane, C. [1 ]
Zazoua, A. [1 ]
Kazane, I. [1 ]
Jaffrezic-Renault, N. [2 ]
机构：
[1] Univ Jijel, Lab Mat Elaborat Proprietes Applicat, Ouled Aissa 18000, Jijel, Algeria
[2] Univ Lyon 1, LSA UMR CNRS 5180, F-69622 Villeurbanne, France
来源：
MATERIALS SCIENCE & ENGINEERING C-MATERIALS FOR BIOLOGICAL APPLICATIONS | 2013年 / 33卷 / 07期
关键词：
Calix[8]arene; Cadmium-sensitive electrode; Impedance spectroscopy; Sensors; ISFET SENSORS; ION DETECTION; THIN-FILMS; CALIXARENE; SPECTROMETRY; CHEMOSENSOR; FLUORESCENT; MERCURY(II); MEMBRANE; PROSTATE;
D O I：
10.1016/j.msec.2013.04.049
中图分类号：
TB3 [工程材料学]; R318.08 [生物材料学];
学科分类号：
0805 ; 080501 ; 080502 ;
摘要：
The performance of a cadmium-sensitive electrode based on the tetracetone derivatives of p-tert butylcalix [8]arene was investigated. The ion-sensitivity of the calix[8]arene was examined via cyclic voltammetry (CV), electrochemical impedance spectroscopy (EIS), X-ray photoelectron spectrometry, UV/Vis spectroscopy and FT-IR spectroscopy. The sensitive membrane containing the active ionophore was cast onto the surface of a gold electrode. The electrode exhibited a linear relationship between the charge transfer resistance (R-ct) and the logarithm of the detected ion concentration. The cathodic peak at a potential of 0.56 V increased linearly as the Cd2+ ion concentration increased. The detection limit of the device reached 10(-7) M with high sensitivity toward cadmium. (C) 2013 Elsevier B.V. All rights reserved.
引用
收藏
页码：3638 / 3643
页数：6
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