Synthesis of some hydroxymethyl derivatives of 4H-pyran-4-ones via N-O bond cleavage

被引:0
|
作者
Teimuri-Mofrad, Reza [1 ]
Abrishami, Fatemeh [1 ]
机构
[1] Malek Ashtar Univ Technol, Dept Chem, Fac Mat, Tehran, Iran
关键词
4H-pyran-4-ones; phthalimidoxymethyl derivatives; hydroxymethyl;
D O I
暂无
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
A new method was developed for the synthesis of hydroxymethyl derivatives of 4H-pyran-4-ones from corresponding phthalimidoxymethyl derivatives by reduction of N-O bond with zinc powder and hydrochloric acid. These phthalimidoxymethyl derivatives of 4H-pyran-4-ones were synthesized by means of reactions of their bromomethyl derivatives and N-hydroxyphthalimide.
引用
收藏
页码:1203 / 1210
页数:8
相关论文
共 50 条
  • [1] Synthesis of some aldoxime derivatives of 4H-pyran-4-ones
    Abrishami, F
    Teimuri-Mofrad, R
    Bayat, Y
    Shahrisa, A
    MOLECULES, 2002, 7 (02) : 239 - 244
  • [2] PHOTOISOMERIZATION OF 4H-PYRAN-4-ONES TO 2H-PYRAN-2-ONES
    ISHIBE, N
    SUNAMI, M
    ODANI, M
    JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1973, 95 (02) : 463 - 468
  • [3] PHOTOCHEMICAL REARRANGEMENT OF 4H-PYRAN-4-ONES TO 2H-PYRAN-2-ONES
    ISHIBE, N
    ODANI, M
    SUNAMI, M
    JOURNAL OF THE CHEMICAL SOCIETY D-CHEMICAL COMMUNICATIONS, 1971, (17): : 1034 - &
  • [4] New podand derivatives of 4H-pyran-4-ones possessing sulfur atoms
    Shahrisa, Aziz
    Mohajery, Shabnam
    Hasanzadeh, Kumarth
    ASIAN JOURNAL OF CHEMISTRY, 2007, 19 (02) : 999 - 1003
  • [5] An efficient synthesis of reduced flavones via Diels-Alder addition to 4H-pyran-4-ones
    Groundwater, PW
    Hibbs, DE
    Hursthouse, MB
    Nyerges, M
    HETEROCYCLES, 1996, 43 (04) : 745 - 749
  • [6] Synthesis and Some Properties of New 5-Hydroxy-2-[(hetarylthio)methyl]-4H-pyran-4-ones
    V. V. Dotsenko
    D. D. Guz
    D. T. Tebiev
    V. K. Kindop
    N. A. Aksenov
    I. V. Aksenova
    E. E. Netreba
    Russian Journal of General Chemistry, 2021, 91 : 1629 - 1638
  • [7] Synthesis and Some Properties of New 5-Hydroxy-2-[(hetarylthio)methyl]-4H-pyran-4-ones
    Dotsenko, V. V.
    Guz, D. D.
    Tebiev, D. T.
    Kindop, V. K.
    Aksenov, N. A.
    Aksenova, I., V
    Netreba, E. E.
    RUSSIAN JOURNAL OF GENERAL CHEMISTRY, 2021, 91 (09) : 1629 - 1638
  • [8] Chemistry of pyrones:: Part 1 -: Synthesis of triketones and triketoesters and related 4H-pyran-4-ones
    Shahrisa, A
    Hemmati, S
    INDIAN JOURNAL OF CHEMISTRY SECTION B-ORGANIC CHEMISTRY INCLUDING MEDICINAL CHEMISTRY, 2000, 39 (03): : 190 - 197
  • [9] Microwave-assisted one-pot synthesis of symmetrical 4H-pyran-4-ones
    Moghaddam, Firouz Matloubi
    Bardajee, Ghasem Rezanejade
    Ismaili, Hossein
    JOURNAL OF THE BRAZILIAN CHEMICAL SOCIETY, 2007, 18 (05) : 1024 - 1027
  • [10] Chemistry of pyrones, part 3:: New podands of 4H-pyran-4-ones
    Shahrisa, A
    Banaei, A
    MOLECULES, 2000, 5 (03) : 200 - 207