Bioanalytical challenge: A review of environmental and pharmaceuticals contaminants in human milk

被引：18
作者：
Lopes, Bianca Rebelo [1 ]
Barreiro, Juliana Cristina [1 ]
Cass, Quezia Bezerra [1 ]
机构：
[1] Univ Fed Sao Carlos, Dept Quim, SEPARARE Nucleo Pesquisa Cromatog, Caixa Postal 676, BR-13565905 Sao Carlos, SP, Brazil
来源：
JOURNAL OF PHARMACEUTICAL AND BIOMEDICAL ANALYSIS | 2016年 / 130卷
基金：
巴西圣保罗研究基金会;
关键词：
Breast milk; Sample preparation; Xenobiotics; Liquid chromatography; Tandem mass spectrometry; HUMAN BREAST-MILK; PERFORMANCE LIQUID-CHROMATOGRAPHY; TANDEM MASS-SPECTROMETRY; BROMINATED FLAME RETARDANTS; RESTRICTED-ACCESS MEDIA; ANTIRETROVIRAL DRUG CONCENTRATIONS; ULTRASOUND-ASSISTED EXTRACTION; ENDOCRINE DISRUPTING CHEMICALS; SAMPLE PREPARATION TECHNIQUES; GREEN ANALYTICAL-CHEMISTRY;
D O I：
10.1016/j.jpba.2016.06.012
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
An overview of bioanalytical methods for the determination of environmental and pharmaceutical contaminants in human milk is presented. The exposure of children to these contaminants through lactation has been widely investigated. The human milk contains diverse proteins, lipids, and carbohydrates and the concentration of these components is drastically altered during the lactation period providing a high degree of an analytical challenge. Sample collection and pretreatment are still considered the Achilles' heel. This review presents liquid chromatographic methods developed in the last 10 years for this complex matrix with focuses in the extraction and quantification steps. Green sample preparation protocols have been emphasized. (C) 2016 Elsevier B.V. All rights reserved.
引用
收藏
页码：318 / 325
页数：8
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