X-ray micro computed tomography characterization of cellular SiC foams for their applications in chemical engineering

被引:47
作者
Ou, Xiaoxia [1 ]
Zhang, Xun [2 ]
Lowe, Tristan [2 ]
Blanc, Remi [3 ]
Rad, Mansoureh Norouzi [1 ]
Wang, Ying [2 ]
Batail, Nelly [4 ]
Pham, Charlotte [4 ]
Shokri, Nima [1 ]
Garforth, Arthur A. [1 ]
Withers, Philip J. [2 ]
Fan, Xiaolei [1 ]
机构
[1] Univ Manchester, Sch Chem Engn & Analyt Sci, Manchester M13 9PL, Lancs, England
[2] Univ Manchester, Sch Mat, Ctr Mat Sci, Henry Moseley Xray Imaging Facil, Manchester M13 9PL, Lancs, England
[3] FEI, 3 Impasse Rudolf Diesel,BP 50227, F-33708 Merignac, France
[4] SICAT SARL, 20 Pl Halles, F-67000 Strasbourg, France
基金
英国工程与自然科学研究理事会;
关键词
Open-cell foam; SiC; X-ray micro computed tomography (mu-CT); Morphometric parameters; Transport properties; Static liquid hold-up; PRESSURE-DROP MEASUREMENTS; STATIC LIQUID HOLDUP; POROUS MATERIALS; METAL FOAMS; FLUID-FLOW; NUMERICAL SIMULATIONS; TRANSPORT-PROPERTIES; SILICON-CARBIDE; DIMETHYL ETHER; CERAMIC FOAMS;
D O I
10.1016/j.matchar.2016.11.013
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Open-cell SiC foams clearly are promising materials for continuous-flow chemical applications such as heterogeneous catalysis and distillation. X-ray micro computed tomography characterization of cellular beta-SiC foams at a spatial voxel size of 13.6(3) mu m(3) and the interpretation of morphological properties of SiC open-cell foams with implications to their transport properties are presented. Static liquid hold-up in SiC foams was investigated through in-situ draining experiments for the first time using the mu-CT technique providing thorough 3D information about the amount and distribution of liquid hold-up inside the foam. This will enable better modeling and design of structured reactors based on SiC foams in the future. In order to see more practical uses, mu-CT data of cellular foams must be exploited to optimize the design of the morphology of foams for a specific application. (C) 2016 Elsevier Inc. All rights reserved.
引用
收藏
页码:20 / 28
页数:9
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