X-ray powder diffraction data and crystal data of polymorphic form 2 of carnidazole

被引:1
作者
de Armas, HN
Peeters, OM
Blaton, N
De Ridder, DJA
Schenk, H
机构
[1] Katholieke Univ Leuven, Fac Farmaceut Wetenschappen, Lab Analyt Chem & Med Fysicochem, B-3000 Louvain, Belgium
[2] Univ Amsterdam, Lab Kristallog, IMC, NL-1018 XE Amsterdam, Netherlands
关键词
X-ray powder diffraction; carnidazole; polymorphism; indexing;
D O I
10.1154/1.2040457
中图分类号
TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
The indexed powder diffraction pattern and related crystallographic data for polymorphic form 2 of carnidazole (C8H12N4O3S) are reported, as a first step in the structure determination by powder diffraction methods. The unit cell dimensions were determined from high resolution synchrotron powder diffraction data (lambda=0.079 998 0 nm) and evaluated by indexing programs. The monoclinic cell found for this polymorph is a=1.3908(2) nm, b=08094(2) nm, c=1.0645(2) nm, beta=110.82(2)degrees, V=1.12015(27) nm(3), Z=4, Dx=1.445 Mg/m(3). (c) 2006 International Centre for Diffraction Data.
引用
收藏
页码:56 / 58
页数:3
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