Quantitative relationship between electrospinning parameters and starch fiber diameter

被引:87
作者
Kong, Lingyan [1 ]
Ziegler, Gregory R. [1 ]
机构
[1] Penn State Univ, Dept Food Sci, University Pk, PA 16802 USA
关键词
Starch; Fiber; Diameter; Electrospinning; Empirical modeling; Response surface methodology; RESPONSE-SURFACE METHODOLOGY; PROCESS OPTIMIZATION; SPUN;
D O I
10.1016/j.carbpol.2012.09.026
中图分类号
O69 [应用化学];
学科分类号
081704 ;
摘要
The diameter of the starch fibers produced by electrospinning is a key parameter for most potential applications. In this study, a quantitative relationship between fiber diameter and certain electrospinning parameters, i.e. starch concentration, applied voltage, spinning distance and feed rate, was established by empirical modeling using a fractional factorial experimental design in a constrained region. Response surface methodology was employed to analyze the interactions of the electrospinning parameters and predict the direction to minimize and maximize the fiber diameters. (C) 2012 Elsevier Ltd. All rights reserved.
引用
收藏
页码:1416 / 1422
页数:7
相关论文
共 12 条
[1]   Process optimization and empirical modeling for electrospun poly(D,L-lactide) fibers using response surface methodology [J].
Gu, SY ;
Ren, J .
MACROMOLECULAR MATERIALS AND ENGINEERING, 2005, 290 (11) :1097-1105
[2]   Process optimization and empirical modeling for electrospun polyacrylonitrile (PAN) nanofiber precursor of carbon nanofibers [J].
Gu, SY ;
Ren, J ;
Vancso, GJ .
EUROPEAN POLYMER JOURNAL, 2005, 41 (11) :2559-2568
[3]  
Kattamuri N., 2004, MACROMOLECULES, V3, P425, DOI DOI 10.1021/MA0351569
[4]  
Kong L., FABRICATION STARCH F
[5]  
Kong L., 2012, RECENT PATENTS FOOD
[6]   Role of Molecular Entanglements in Starch Fiber Formation by Electrospinning [J].
Kong, Lingyan ;
Ziegler, Gregory R. .
BIOMACROMOLECULES, 2012, 13 (08) :2247-2253
[7]  
Kong LY, 2010, POLYM SCI TECHNOL SE, P1
[8]   Dry-Jet-Wet Spun Polyurethane Fibers. I. Optimization of the Spinning Parameters [J].
Reddy, G. V. Raghunath ;
Deopura, B. L. ;
Joshi, Mangala .
JOURNAL OF APPLIED POLYMER SCIENCE, 2010, 118 (04) :2291-2303
[9]   Transport properties of electrospun nylon 6 nonwoven mats [J].
Ryu, YJ ;
Kim, HY ;
Lee, KH ;
Park, HC ;
Lee, DR .
EUROPEAN POLYMER JOURNAL, 2003, 39 (09) :1883-1889
[10]   Regeneration of Bombyx mori silk by electrospinning.: Part 2.: Process optimization and empirical modeling using response surface methodology [J].
Sukigara, S ;
Gandhi, M ;
Ayutsede, J ;
Micklus, M ;
Ko, F .
POLYMER, 2004, 45 (11) :3701-3708