Effect of a pre-aging treatment on the mechanical behaviors of Ni50.3Ti49.7 - xHfx (x ≤ 9 at.%) Shape memory alloys

被引:27
作者
Amin-Ahmadi, Behnam [1 ]
Gallmeyer, Thomas [1 ]
Pauza, Joseph G. [1 ]
Duerig, Tom W. [2 ]
Noebe, Ronald D. [3 ]
Stebner, Aaron P. [1 ]
机构
[1] Colorado Sch Mines, Mech Engn, Golden, CO 80401 USA
[2] Confluent Med Technol, Fremont, CA 94539 USA
[3] NASA, Glenn Res Ctr, Mat & Struct Div, Cleveland, OH 44135 USA
关键词
Aging; NiTiHf shape memory alloy; Transmission electron microscopy (TEM); Precipitation; H-phase; Superelasticity; NI-RICH NITIHF; PRECIPITATE PHASE;
D O I
10.1016/j.scriptamat.2017.12.024
中图分类号
TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
Transmission electron microscopy and mechanical testing were used to determine the effect of pre-aging (300 degrees C for 12 h) on microstructure and mechanical behavior of a series of Ni50.3Ti49.7 - xHfx, shape memory alloys (x = 6, 8, 8.5, 9 at.%) prior to normal aging at 550 degrees C for 3.5 h. Pre-aging was found to promote homogenous nucleation of nanosized H-phase precipitates, resulting in improved mechanical stability and strength and 4% recoverable compression strain without permanent deformation. The absence of pre-aging generally resulted in heterogeneous formations of larger H-phase precipitates, primarily clustered along grain boundaries, and correlated with poorer mechanical behavior. (C) 2017 Acta Materialia Inc. Published by Elsevier Ltd. All rights reserved.
引用
收藏
页码:11 / 15
页数:5
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