Preliminary evaluation of laser induced breakdown spectroscopy for slurry samples

被引：32

作者：

Oh, Seong Yong ^{[1
]}

Yueh, Fang Yu ^{[1
]}

Singh, Jagdish P. ^{[1
]}

Herman, Connie C. ^{[2
]}

Zeigler, Kristine ^{[2
]}

机构：

[1] Mississippi State Univ, Inst Clean Energy Technol, Starkville, MS 39759 USA

[2] Savannah River Natl Lab, Aiken, SC 29808 USA

来源：

SPECTROCHIMICA ACTA PART B-ATOMIC SPECTROSCOPY | 2009年 / 64卷 / 01期

关键词：

Slurry; Laser induced breakdown spectroscopy; Echelle spectrometer; Czerny-Turner spectrometer; INDUCED PLASMA SPECTROSCOPY; BOTTOM ASHES; GLASS MELTS; VITRIFICATION; SPECTROMETRY; FLY;

D O I：

10.1016/j.sab.2008.10.023

中图分类号：

O433 [光谱学];

学科分类号：

0703 ; 070302 ;

摘要：

Laser-induced breakdown spectroscopy (LIBS) was applied to the analysis of simulant slurry samples used in the vitrification process of liquid radioactive wastes. A spectroscopic analysis was performed by two different detection systems: Czerny-Turner spectrometer coupled with intensified diode array detector (IDAD) and an Echelle spectrometer with intensified charge coupled device (ICCD). For the Czerny-Turner detection system. the normalized intensity method, which is the normalization of the atomic emission intensity by the released whole plasma emission area intensity. was employed to improve the reproducibility of LIBS signals. The Echelle detection system showed a high efficiency in simultaneous multi-element detection and determination of the physical quantities of the simulant. (C) 2008 Elsevier B.V. All rights reserved.

引用

页码：113 / 118

页数：6

共 25 条

[21]

WINEFORDNER JD, 2000, 9604057R FIRP U FLOR

[22] Evaluation of the potential of laser-induced breakdown spectroscopy for detection of trace element in liquid [J].

Yueh, FY ;

Sharma, RC ;

Singh, JP ;

Zhang, HS ;

Spencer, WA .

JOURNAL OF THE AIR & WASTE MANAGEMENT ASSOCIATION, 2002, 52 (11) :1307-1315

[23]

YUEH FY, 2000, ENCY ANAL CHEM, P2065

[24] Laser-induced breakdown spectroscopy for the on-line multielement analysis of highly radioactive glass melt. Part 1: Characterization and evaluation of the method [J].

Yun, JI ;

Klenze, R ;

Kim, JI .

APPLIED SPECTROSCOPY, 2002, 56 (04) :437-448

[25]

ZHANG H, 2001, J AIR WASTE MANAGE, V51, P174

← 1 2 3 →