A facile route for the preparation of silica foams using rice husk ash

被引:27
作者
Hossain, S. K. Saddam [1 ]
Mathur, Lakshya [1 ]
Bhardwaj, Aman [1 ]
Roy, Pradip Kumar [1 ]
机构
[1] IIT BHU, Dept Ceram Engn, Varanasi, Uttar Pradesh, India
关键词
foams; porous materials; rice husk ash; silica; waste disposal; HIGH-SURFACE-AREA; AMORPHOUS SILICA; PORE-SIZE; CERAMICS; NANOPARTICLES; MICROSPHERES; EXTRACTION; NANOWIRES; ALUMINA; ACID;
D O I
10.1111/ijac.13164
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
This work aims to synthesize silica foam with around 75 vol. % open porosity without using any additive or pore forming agents, in order to prevent the generation of greenhouse gases during pore formation in the silica matrix. Waste rice husk ash (RHA) derived silica is used as a silica source, which is extracted through the alkali extraction synthesis route. Several physical characterizations such as X-ray diffraction (XRD), scanning electron microscope (SEM), transmission electron microscopy (TEM), differential thermal-thermogravimetric (DTA-TGA) and FTIR analysis have been done for RHA extracted silica. Silica foam specimens are fabricated through control compaction pressure and at low foaming temperature. Samples which are fired at 550 degrees C for 30 minutes exhibit both a adequate apparent porosity (AP; similar to 75.82%) and significant compressive strength (similar to 1.54 MPa). It can also be observed that the porosity and strength values are changed with the variation in compaction pressure and foaming temperature.
引用
收藏
页码:1069 / 1077
页数:9
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