Nickel oxide nanoparticles: Synthesis and spectral studies of interactions with glucose

被引:533
作者
El-Kemary, M. [1 ]
Nagy, N. [1 ]
El-Mehasseb, I. [1 ]
机构
[1] Kafrelsheikh Univ, Fac Sci, Dept Chem, Nanochem Lab, Kafr Al Sheikh 33516, Egypt
关键词
Nickel oxide; Nanoparticles; Glucose; Fluorescence; THIN-FILMS; NIO; NI(OH)(2); ARRAYS;
D O I
10.1016/j.mssp.2013.05.018
中图分类号
TM [电工技术]; TN [电子技术、通信技术];
学科分类号
0808 ; 0809 ;
摘要
Nickel oxide (NiO) nanoparticles were successfully synthesized by the reaction of nickel chloride with hydrazine at room temperature and thermal decomposition of the precursor nickel hydroxide (Ni(OH)(2)) nanoparticles. The products were characterized by X-ray diffraction, Transmission electron microscopy, Fourier transform infrared spectroscopy, and UV-vis absorption spectroscopy. The result of thermogravimetric analysis showed that the Ni(OH)(2) nanoparticles are calcinated at similar to 400 degrees C. The interactions between NiO nanoparticles and glucose have been studied using UV-vis absorption and fluorescence spectroscopy. The zeta-potential of NiO nanoparticles was used to gain insight about the interaction mode between NiO nanoparticles and glucose. (C) 2013 The authors. Published by Elsevier Ltd. All rights reserved.
引用
收藏
页码:1747 / 1752
页数:6
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